3-(4-tert-butylbenzoyl)-2,7-dibromo-N-(2-ethylhexyl)carbazole

Base Information

• Chemical Name: 3-(4-tert-butylbenzoyl)-2,7-dibromo-N-(2-ethylhexyl)carbazole
• CAS No.: 862493-92-3
• Molecular Formula: C₃₁H₃₅Br₂NO
• Molecular Weight: 597.433
• Mol file: 862493-92-3.mol

Synonyms:3-(4-tert-butylbenzoyl)-2,7-dibromo-N-(2-ethylhexyl)carbazole

Chemical Property of 3-(4-tert-butylbenzoyl)-2,7-dibromo-N-(2-ethylhexyl)carbazole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-(4-tert-butylbenzoyl)-2,7-dibromo-N-(2-ethylhexyl)carbazole

There total 3 articles about 3-(4-tert-butylbenzoyl)-2,7-dibromo-N-(2-ethylhexyl)carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

p-tert-butyl benzoyl chloride (1710-98-1) + 2,7-dibromo-9-(2-ethyl-hexyl)-9H-carbazole (544436-46-6) → 3-(4-tert-butylbenzoyl)-2,7-dibromo-N-(2-ethylhexyl)carbazole (862493-92-3)

Guidance literature:

With aluminium trichloride; In 1,2-dichloro-ethane; at 20 ℃; for 8h;

DOI:10.1021/ma050821u

Reference yield:

3-bromomethylheptane (18908-66-2) → 3-(4-tert-butylbenzoyl)-2,7-dibromo-N-(2-ethylhexyl)carbazole (862493-92-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 78 percent / K₂CO₃ / dimethylformamide / 24 h / 80 °C

2: 70 percent / AlCl₃ / 1,2-dichloro-ethane / 8 h / 20 °C

With aluminium trichloride; potassium carbonate; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;

DOI:10.1021/ma050821u

Reference yield:

2,7-dibromo-9H-carbazole (136630-39-2) → 3-(4-tert-butylbenzoyl)-2,7-dibromo-N-(2-ethylhexyl)carbazole (862493-92-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 78 percent / K₂CO₃ / dimethylformamide / 24 h / 80 °C

2: 70 percent / AlCl₃ / 1,2-dichloro-ethane / 8 h / 20 °C

With aluminium trichloride; potassium carbonate; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;

DOI:10.1021/ma050821u

upstream raw materials:

p-tert-butyl benzoyl chloride

2,7-dibromo-9-(2-ethyl-hexyl)-9H-carbazole

3-bromomethylheptane

2,7-dibromo-9H-carbazole