Technology Process of C31H31BF2N4OSi
There total 5 articles about C31H31BF2N4OSi which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine;
In
tetrahydrofuran; toluene;
at 20 ℃;
for 2h;
Inert atmosphere;
DOI:10.1039/c3cc41555d
- Guidance literature:
-
Multi-step reaction with 2 steps
1: boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine / 1 h / 85 °C
2: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran; toluene / 2 h / 20 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; boron trifluoride diethyl etherate; triethylamine; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; toluene;
DOI:10.1039/c3cc41555d
- Guidance literature:
-
Multi-step reaction with 4 steps
1: piperidine / ethanol / 1 h / Reflux
2: toluene-4-sulfonic acid / ethanol / Reflux
3: boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine / 1 h / 85 °C
4: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran; toluene / 2 h / 20 °C / Inert atmosphere
With
piperidine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; boron trifluoride diethyl etherate; toluene-4-sulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; ethanol; toluene;
DOI:10.1039/c3cc41555d
