2-naphthaldehyde (4-methoxyphenyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-β-D-glucopyranosid-2-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-1-thio-β-D-glucopyranosid-2-yl) acetal

Base Information

Chemical Name:2-naphthaldehyde (4-methoxyphenyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-β-D-glucopyranosid-2-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-1-thio-β-D-glucopyranosid-2-yl) acetal
CAS No.:1075708-71-2
Molecular Formula:C₅₇H₆₆O₁₂S
Molecular Weight:989.099
Hs Code.:

2-naphthaldehyde (4-methoxyphenyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-β-D-glucopyranosid-2-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-1-thio-β-D-glucopyranosid-2-yl) acetal

Synonyms:2-naphthaldehyde (4-methoxyphenyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-β-D-glucopyranosid-2-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-1-thio-β-D-glucopyranosid-2-yl) acetal

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Chemical Property of 2-naphthaldehyde (4-methoxyphenyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-β-D-glucopyranosid-2-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-1-thio-β-D-glucopyranosid-2-yl) acetal

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Technology Process of 2-naphthaldehyde (4-methoxyphenyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-β-D-glucopyranosid-2-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-1-thio-β-D-glucopyranosid-2-yl) acetal

There total 2 articles about 2-naphthaldehyde (4-methoxyphenyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-β-D-glucopyranosid-2-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-1-thio-β-D-glucopyranosid-2-yl) acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 4-methoxyphenyl 3-O-(benzyl-d7)-4,6-O-cyclohexylidene-β-D-glucopyranoside

: 1075708-62-1
methyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-2-O-2-naphthylmethyl-1-thio-β-D-glucopyranoside

: 1075708-71-2
2-naphthaldehyde (4-methoxyphenyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-β-D-glucopyranosid-2-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-1-thio-β-D-glucopyranosid-2-yl) acetal

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 17h; Molecular sieve; Inert atmosphere;
DOI:10.1002/ejoc.200800249

Reference yield: 93.0%

: 1075708-69-8
methyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-1-thio-β-D-glucopyranoside

: 1075708-70-1
4-methoxyphenyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene2-O-(2-naphthylmethyl)-β-D-glucopyranoside

: 1075708-71-2
2-naphthaldehyde (4-methoxyphenyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-β-D-glucopyranosid-2-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-1-thio-β-D-glucopyranosid-2-yl) acetal

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 17h; Molecular sieve; Inert atmosphere;
DOI:10.1002/ejoc.200800249

Reference yield: 85.0%

: 1075708-71-2
2-naphthaldehyde (4-methoxyphenyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-β-D-glucopyranosid-2-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-1-thio-β-D-glucopyranosid-2-yl) acetal

: 1075708-75-6
4-methoxyphenyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->2)-3-O-[D7]benzyl-4,6-O-cyclohexylidene-β-D-glucopyranoside

Guidance literature:: 2-naphthaldehyde (4-methoxyphenyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-β-D-glucopyranosid-2-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-1-thio-β-D-glucopyranosid-2-yl) acetal; With 2,6-di-tert-butyl-4-methylpyridine; tris-(trimethylsilyl)silane; methyl trifluoromethanesulfonate; In 1,2-dichloro-ethane; at 20 ℃; for 17h; Molecular sieve; Inert atmosphere;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In 1,2-dichloro-ethane;
DOI:10.1002/ejoc.200800249