methyl 7-amino-2,3-di-O-benzyl-6,7-dideoxy-4-O-methyl-α-D-glucoheptopyranoside

Base Information

Chemical Name:methyl 7-amino-2,3-di-O-benzyl-6,7-dideoxy-4-O-methyl-α-D-glucoheptopyranoside
CAS No.:193287-59-1
Molecular Formula:C₂₃H₃₁NO₅
Molecular Weight:401.503
Hs Code.:

Synonyms:methyl 7-amino-2,3-di-O-benzyl-6,7-dideoxy-4-O-methyl-α-D-glucoheptopyranoside

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Chemical Property of methyl 7-amino-2,3-di-O-benzyl-6,7-dideoxy-4-O-methyl-α-D-glucoheptopyranoside

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Technology Process of methyl 7-amino-2,3-di-O-benzyl-6,7-dideoxy-4-O-methyl-α-D-glucoheptopyranoside

There total 4 articles about methyl 7-amino-2,3-di-O-benzyl-6,7-dideoxy-4-O-methyl-α-D-glucoheptopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 193287-58-0
methyl 2,3-di-O-benzyl-6-cyano-6-deoxy-4-O-methyl-α-D-glucopyranoside

: 193287-59-1
methyl 7-amino-2,3-di-O-benzyl-6,7-dideoxy-4-O-methyl-α-D-glucoheptopyranoside

Guidance literature:: With ammonia; hydrogen; Rh/Al₂O₃; In methanol; under 37503 Torr;
DOI:10.1016/S0008-6215(97)00091-8

Reference yield:

: 54522-57-5
methyl-2,3-di-O-benzyl-6-O-(4-toluenesulfonyl)-α-D-glucopyranoside

: 193287-59-1
methyl 7-amino-2,3-di-O-benzyl-6,7-dideoxy-4-O-methyl-α-D-glucoheptopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: NaOH / CH₂Cl₂; H₂O / 0 - 20 °C

2: 960 mg / N,N-dimethyl-acetamide / 48 h / 80 °C

3: 91 percent / H₂; NH₃ / 5 percent rhodium on Al₂O₃ / methanol / 37503 Torr

With sodium hydroxide; ammonia; hydrogen; Rh/Al₂O₃; In methanol; dichloromethane; N,N-dimethyl acetamide; water; 1: Methylation / 2: Substitution / 3: Reduction;
DOI:10.1016/S0008-6215(97)00091-8

Reference yield:

: 193287-39-7
methyl 2,3-di-O-benzyl-4-O-methyl-6-O-p-toluenesulfonyl-α-D-glucopyranoside

: 193287-59-1
methyl 7-amino-2,3-di-O-benzyl-6,7-dideoxy-4-O-methyl-α-D-glucoheptopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 960 mg / N,N-dimethyl-acetamide / 48 h / 80 °C

2: 91 percent / H₂; NH₃ / 5 percent rhodium on Al₂O₃ / methanol / 37503 Torr

With ammonia; hydrogen; Rh/Al₂O₃; In methanol; N,N-dimethyl acetamide; 1: Substitution / 2: Reduction;
DOI:10.1016/S0008-6215(97)00091-8