2-Benzyl-5-carboxymethyl-3,4,6-triphenyl-cyclohex-3-enecarboxylic acid

Base Information

• Chemical Name: 2-Benzyl-5-carboxymethyl-3,4,6-triphenyl-cyclohex-3-enecarboxylic acid
• CAS No.: 81555-70-6
• Molecular Formula: C₃₄H₃₀O₄
• Molecular Weight: 502.61
• Mol file: 81555-70-6.mol

Synonyms:2-Benzyl-5-carboxymethyl-3,4,6-triphenyl-cyclohex-3-enecarboxylic acid

Chemical Property of 2-Benzyl-5-carboxymethyl-3,4,6-triphenyl-cyclohex-3-enecarboxylic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Benzyl-5-carboxymethyl-3,4,6-triphenyl-cyclohex-3-enecarboxylic acid

There total 1 articles about 2-Benzyl-5-carboxymethyl-3,4,6-triphenyl-cyclohex-3-enecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

trans-8,8a-dihydro-4,7,8,8a-tetraphenylbenzo<1,2-b:4,5-c'>difuran-2,5-dione (80716-67-2) → 2-Benzyl-5-carboxymethyl-3,4,6-triphenyl-cyclohex-3-enecarboxylic acid (81555-70-6)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate; for 96h; under 2585.7 Torr; Ambient temperature;

DOI:10.1021/jo00134a014

Reference yield: 72.0%

diazomethane (186581-53-3,908094-01-9,334-88-3) + 2-Benzyl-5-carboxymethyl-3,4,6-triphenyl-cyclohex-3-enecarboxylic acid (81555-70-6) → 2-Benzyl-5-methoxycarbonylmethyl-3,4,6-triphenyl-cyclohex-3-enecarboxylic acid methyl ester (81555-71-7)

Guidance literature:

In methanol; diethyl ether; at 0 ℃;

DOI:10.1021/jo00134a014

upstream raw materials:

trans-8,8a-dihydro-4,7,8,8a-tetraphenylbenzo<1,2-b:4,5-c'>difuran-2,5-dione

Downstream raw materials:

2-Benzyl-5-methoxycarbonylmethyl-3,4,6-triphenyl-cyclohex-3-enecarboxylic acid methyl ester