(1S,3aS,5aS,6R,11bR,11cR)-3-benzyl-14-(cyclopropylmethyl)-3a,11-dihydroxy-10-methoxy-1,3,3a,4,5,6,7,11c-octahydro-2H-6,11b-(iminoethano)-1,5a-epoxynaphtho[1,2-e]indol-2-one

Base Information

• Chemical Name: (1S,3aS,5aS,6R,11bR,11cR)-3-benzyl-14-(cyclopropylmethyl)-3a,11-dihydroxy-10-methoxy-1,3,3a,4,5,6,7,11c-octahydro-2H-6,11b-(iminoethano)-1,5a-epoxynaphtho[1,2-e]indol-2-one
• CAS No.: 1331828-01-3
• Molecular Formula: C₃₀H₃₄N₂O₅
• Molecular Weight: 502.61

Synonyms:(1S,3aS,5aS,6R,11bR,11cR)-3-benzyl-14-(cyclopropylmethyl)-3a,11-dihydroxy-10-methoxy-1,3,3a,4,5,6,7,11c-octahydro-2H-6,11b-(iminoethano)-1,5a-epoxynaphtho[1,2-e]indol-2-one

Chemical Property of (1S,3aS,5aS,6R,11bR,11cR)-3-benzyl-14-(cyclopropylmethyl)-3a,11-dihydroxy-10-methoxy-1,3,3a,4,5,6,7,11c-octahydro-2H-6,11b-(iminoethano)-1,5a-epoxynaphtho[1,2-e]indol-2-one

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Technology Process of (1S,3aS,5aS,6R,11bR,11cR)-3-benzyl-14-(cyclopropylmethyl)-3a,11-dihydroxy-10-methoxy-1,3,3a,4,5,6,7,11c-octahydro-2H-6,11b-(iminoethano)-1,5a-epoxynaphtho[1,2-e]indol-2-one

There total 9 articles about (1S,3aS,5aS,6R,11bR,11cR)-3-benzyl-14-(cyclopropylmethyl)-3a,11-dihydroxy-10-methoxy-1,3,3a,4,5,6,7,11c-octahydro-2H-6,11b-(iminoethano)-1,5a-epoxynaphtho[1,2-e]indol-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

C30H34N2O5 (1186029-05-9) → (1S,3aS,5aS,6R,11bR,11cR)-3-benzyl-14-(cyclopropylmethyl)-3a,11-dihydroxy-10-methoxy-1,3,3a,4,5,6,7,11c-octahydro-2H-6,11b-(iminoethano)-1,5a-epoxynaphtho[1,2-e]indol-2-one (1331828-01-3)

Guidance literature:

C₃₀H₃₄N₂O₅; With potassium tert-butylate; In tert-butyl alcohol; for 1h; Inert atmosphere; Reflux;

With hydrogenchloride; In water; tert-butyl alcohol;

DOI:10.1016/j.tet.2011.04.097

Reference yield: 89.0%

C30H34N2O5 (1186029-08-2) → (1S,3aS,5aS,6R,11bR,11cR)-3-benzyl-14-(cyclopropylmethyl)-3a,11-dihydroxy-10-methoxy-1,3,3a,4,5,6,7,11c-octahydro-2H-6,11b-(iminoethano)-1,5a-epoxynaphtho[1,2-e]indol-2-one (1331828-01-3)

Guidance literature:

C₃₀H₃₄N₂O₅; With potassium tert-butylate; In tert-butyl alcohol; for 1h; Inert atmosphere; Reflux;

With hydrogenchloride; In water; tert-butyl alcohol;

DOI:10.1016/j.tet.2011.04.097

Reference yield: 89.0%

(5R,6S,6'S,9R,13S,14S)-N-benzyl-17-(cyclopropylmethyl)-4,5-epoxy-6,6'-epoxy-14-hydroxy-3-methoxy-6-methylmorphinan-6'-carboxamide → (1S,3aS,5aS,6R,11bR,11cR)-3-benzyl-14-(cyclopropylmethyl)-3a,11-dihydroxy-10-methoxy-1,3,3a,4,5,6,7,11c-octahydro-2H-6,11b-(iminoethano)-1,5a-epoxynaphtho[1,2-e]indol-2-one (1331828-01-3)

Guidance literature:

With potassium tert-butylate; In tert-butyl alcohol; for 1h; Inert atmosphere; Reflux;

upstream raw materials:

C₂₅H₃₁NO₆

(5R,6S,7S,9R,13S,14S)-N-benzyl-17-(cyclopropylmethyl)-4,5-epoxy-6-hydroxy-3-methoxy-8-oxa-6,14-ethanomorphinan-7-carboxamide

C₃₀H₃₄N₂O₅

C₃₀H₃₄N₂O₅

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