3-(1-adamantyl)-4-<<(2,3-dimethyl-1,3-dioxolan-4-yl)methyl>oxy>bromobenzene

Base Information

Chemical Name:3-(1-adamantyl)-4-<<(2,3-dimethyl-1,3-dioxolan-4-yl)methyl>oxy>bromobenzene
CAS No.:146966-00-9
Molecular Formula:C₂₂H₂₉BrO₃
Molecular Weight:421.374
Hs Code.:

Synonyms:3-(1-adamantyl)-4-<<(2,3-dimethyl-1,3-dioxolan-4-yl)methyl>oxy>bromobenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(1-adamantyl)-4-<<(2,3-dimethyl-1,3-dioxolan-4-yl)methyl>oxy>bromobenzene

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Technology Process of 3-(1-adamantyl)-4-<<(2,3-dimethyl-1,3-dioxolan-4-yl)methyl>oxy>bromobenzene

There total 4 articles about 3-(1-adamantyl)-4-<<(2,3-dimethyl-1,3-dioxolan-4-yl)methyl>oxy>bromobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 104224-68-2
2-(1-adamantyl)-4-bromophenol

: 23737-51-1,7305-59-1
solketal tosylate

: 146966-00-9
3-(1-adamantyl)-4-<<(2,3-dimethyl-1,3-dioxolan-4-yl)methyl>oxy>bromobenzene

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 12h;
DOI:10.1021/jm00026a006

Reference yield:

: 106-41-2
4-bromo-phenol

: 146966-00-9
3-(1-adamantyl)-4-<<(2,3-dimethyl-1,3-dioxolan-4-yl)methyl>oxy>bromobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / conc. H₂SO₄ / CH₂Cl₂ / 8 h / Ambient temperature

2: 55 percent / K₂CO₃ / dimethylformamide / 12 h / 100 °C

With sulfuric acid; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00026a006

Reference yield:

: 768-95-6
1-adamanthanol

: 146966-00-9
3-(1-adamantyl)-4-<<(2,3-dimethyl-1,3-dioxolan-4-yl)methyl>oxy>bromobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / conc. H₂SO₄ / CH₂Cl₂ / 8 h / Ambient temperature

2: 55 percent / K₂CO₃ / dimethylformamide / 12 h / 100 °C

With sulfuric acid; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00026a006