Acetic acid 1-[5-(tert-butyl-dimethyl-silanyl)-furan-3-yl]-11-phenyl-undecyl ester

Base Information

• Chemical Name: Acetic acid 1-[5-(tert-butyl-dimethyl-silanyl)-furan-3-yl]-11-phenyl-undecyl ester
• CAS No.: 136617-91-9
• Molecular Formula: C₂₉H₄₆O₃Si
• Molecular Weight: 470.768

Synonyms:Acetic acid 1-[5-(tert-butyl-dimethyl-silanyl)-furan-3-yl]-11-phenyl-undecyl ester

Chemical Property of Acetic acid 1-[5-(tert-butyl-dimethyl-silanyl)-furan-3-yl]-11-phenyl-undecyl ester

Chemical Property:

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Technology Process of Acetic acid 1-[5-(tert-butyl-dimethyl-silanyl)-furan-3-yl]-11-phenyl-undecyl ester

There total 3 articles about Acetic acid 1-[5-(tert-butyl-dimethyl-silanyl)-furan-3-yl]-11-phenyl-undecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[4-(6-Bromohexyl)butyl]benzene (85562-26-1) → Acetic acid 1-[5-(tert-butyl-dimethyl-silanyl)-furan-3-yl]-11-phenyl-undecyl ester (136617-91-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) Mg / 1.) THF, 2.) 0 deg C, THF

2: tetrahydrofuran / Ambient temperature

With magnesium; In tetrahydrofuran;

DOI:10.1021/jo00025a012

Reference yield:

2-(tert-butyldimethylsilyl)-4-furaldehyde (130493-23-1) → Acetic acid 1-[5-(tert-butyl-dimethyl-silanyl)-furan-3-yl]-11-phenyl-undecyl ester (136617-91-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) Mg / 1.) THF, 2.) 0 deg C, THF

2: tetrahydrofuran / Ambient temperature

With magnesium; In tetrahydrofuran;

DOI:10.1021/jo00025a012

Reference yield:

acetic anhydride (108-24-7) + 1-[5-(tert-Butyl-dimethyl-silanyl)-furan-3-yl]-11-phenyl-undecan-1-ol → Acetic acid 1-[5-(tert-butyl-dimethyl-silanyl)-furan-3-yl]-11-phenyl-undecyl ester (136617-91-9)

Guidance literature:

In tetrahydrofuran; Yield given; Ambient temperature;

DOI:10.1021/jo00025a012

upstream raw materials:

acetic anhydride

[4-(6-Bromohexyl)butyl]benzene

2-(tert-butyldimethylsilyl)-4-furaldehyde

Downstream raw materials:

4-(1-Acetoxy-11-phenylundecyl)-5-hydroxy-2(5H)-furanone

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