(S)-3-Benzyloxycarbonylamino-N-[phenyl-(2,2,5,5-tetramethyl-cyclopentyloxycarbonyl)-methyl]-succinamic acid benzyl ester

Base Information

Chemical Name:(S)-3-Benzyloxycarbonylamino-N-[phenyl-(2,2,5,5-tetramethyl-cyclopentyloxycarbonyl)-methyl]-succinamic acid benzyl ester
CAS No.:124441-94-7
Molecular Formula:C₃₆H₄₂N₂O₇
Molecular Weight:614.739
Hs Code.:

Synonyms:(S)-3-Benzyloxycarbonylamino-N-[phenyl-(2,2,5,5-tetramethyl-cyclopentyloxycarbonyl)-methyl]-succinamic acid benzyl ester

Suppliers and Price of (S)-3-Benzyloxycarbonylamino-N-[phenyl-(2,2,5,5-tetramethyl-cyclopentyloxycarbonyl)-methyl]-succinamic acid benzyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-3-Benzyloxycarbonylamino-N-[phenyl-(2,2,5,5-tetramethyl-cyclopentyloxycarbonyl)-methyl]-succinamic acid benzyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (S)-3-Benzyloxycarbonylamino-N-[phenyl-(2,2,5,5-tetramethyl-cyclopentyloxycarbonyl)-methyl]-succinamic acid benzyl ester

There total 4 articles about (S)-3-Benzyloxycarbonylamino-N-[phenyl-(2,2,5,5-tetramethyl-cyclopentyloxycarbonyl)-methyl]-succinamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15231-50-2
2,2,5,5-tetramethyl-1-cyclopentanol

: 124441-94-7
(S)-3-Benzyloxycarbonylamino-N-[phenyl-(2,2,5,5-tetramethyl-cyclopentyloxycarbonyl)-methyl]-succinamic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / CH₂Cl₂ / 1.) -78 deg C, 0.5 h, 2.) -23 deg C

2: 5N HCl / acetone

3: tetrahydrofuran / 24 h

With hydrogenchloride; dmap; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1021/jm00165a027

Reference yield:

: 875-74-1
(R)-phenylglycine

: 124441-94-7
(S)-3-Benzyloxycarbonylamino-N-[phenyl-(2,2,5,5-tetramethyl-cyclopentyloxycarbonyl)-methyl]-succinamic acid benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 62 percent / 2N NaOH / dioxane / 2 h

2: dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / CH₂Cl₂ / 1.) -78 deg C, 0.5 h, 2.) -23 deg C

3: 5N HCl / acetone

4: tetrahydrofuran / 24 h

With hydrogenchloride; dmap; sodium hydroxide; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; acetone;
DOI:10.1021/jm00165a027

Reference yield:

: 16679-41-7
N-<(o-nitrophenyl)sulfenyl>-D-phenylglycine

: 124441-94-7
(S)-3-Benzyloxycarbonylamino-N-[phenyl-(2,2,5,5-tetramethyl-cyclopentyloxycarbonyl)-methyl]-succinamic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / CH₂Cl₂ / 1.) -78 deg C, 0.5 h, 2.) -23 deg C

2: 5N HCl / acetone

3: tetrahydrofuran / 24 h

With hydrogenchloride; dmap; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1021/jm00165a027