phenylbis(5,6-dimethyl-7-phenyl-7-phosphabicyclo{2.2.1}hept-5-en-2-yl)phosphine

Base Information

Chemical Name:phenylbis(5,6-dimethyl-7-phenyl-7-phosphabicyclo{2.2.1}hept-5-en-2-yl)phosphine
CAS No.:121920-79-4
Molecular Formula:C₃₄H₃₇P₃
Molecular Weight:538.589
Hs Code.:

Synonyms:phenylbis(5,6-dimethyl-7-phenyl-7-phosphabicyclo{2.2.1}hept-5-en-2-yl)phosphine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenylbis(5,6-dimethyl-7-phenyl-7-phosphabicyclo{2.2.1}hept-5-en-2-yl)phosphine

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Technology Process of phenylbis(5,6-dimethyl-7-phenyl-7-phosphabicyclo{2.2.1}hept-5-en-2-yl)phosphine

There total 1 articles about phenylbis(5,6-dimethyl-7-phenyl-7-phosphabicyclo{2.2.1}hept-5-en-2-yl)phosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 121935-47-5
bromo{phenylbis(5,6-dimethyl-7-phenyl-7-phosphabicyclo{2.2.1}hept-5-en-2-yl)phosphine}nickel(II) bromide-dichloromethane

: 121920-79-4
phenylbis(5,6-dimethyl-7-phenyl-7-phosphabicyclo{2.2.1}hept-5-en-2-yl)phosphine

Guidance literature:: With NaCN; In dichloromethane; water; Addn. of satd. aq. NaCN soln. to Ni-complex in CH2Cl2 under N2, vigorous stirring (room temp, 45 min).; Sepg. of CH2Cl2 layer, filtn., concg., addn. of EtOH gives colorless crystals, elem. anal.;
DOI:10.1021/ic00317a012