(1RS,5RS,12SR)-benzyl 12-ethyl-6-oxo-1,2,3,4,5,6-hexahydro-1,5-methanoazocino[4,3-b]indole-carboxylate

Base Information

Chemical Name:(1RS,5RS,12SR)-benzyl 12-ethyl-6-oxo-1,2,3,4,5,6-hexahydro-1,5-methanoazocino[4,3-b]indole-carboxylate
CAS No.:139750-89-3
Molecular Formula:C₂₄H₂₄N₂O₃
Molecular Weight:388.466
Hs Code.:

Synonyms:(1RS,5RS,12SR)-benzyl 12-ethyl-6-oxo-1,2,3,4,5,6-hexahydro-1,5-methanoazocino[4,3-b]indole-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1RS,5RS,12SR)-benzyl 12-ethyl-6-oxo-1,2,3,4,5,6-hexahydro-1,5-methanoazocino[4,3-b]indole-carboxylate

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Technology Process of (1RS,5RS,12SR)-benzyl 12-ethyl-6-oxo-1,2,3,4,5,6-hexahydro-1,5-methanoazocino[4,3-b]indole-carboxylate

There total 7 articles about (1RS,5RS,12SR)-benzyl 12-ethyl-6-oxo-1,2,3,4,5,6-hexahydro-1,5-methanoazocino[4,3-b]indole-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 139758-45-5
C₂₄H₂₆N₂O₂

: 139750-89-3
(1RS,5RS,12SR)-benzyl 12-ethyl-6-oxo-1,2,3,4,5,6-hexahydro-1,5-methanoazocino[4,3-b]indole-carboxylate

Guidance literature:: With selenium(IV) oxide; In 1,4-dioxane; at 80 ℃; for 40h;
DOI:10.1039/c39910001687

Reference yield:

: 1075724-76-3
phenyl 3-[1-(benzyloxycarbonyl)-3-ethyl-1,2,5,6-tetrahydro-2-pyridyl]indole-2-carboselenoate

: benzyl 4a-ethyl-3,4,4a,5,6,10c-hexahydro-5-oxo-2H-pyrido[2',3':3,4]cyclopenta[1,2-b]indole-1-carboxylate

: 139750-89-3
(1RS,5RS,12SR)-benzyl 12-ethyl-6-oxo-1,2,3,4,5,6-hexahydro-1,5-methanoazocino[4,3-b]indole-carboxylate

Guidance literature:: With triethyl borane; tri-n-butyl-tin hydride; In hexane; benzene; at 20 ℃; for 3h;
DOI:10.1021/jo801998h

Reference yield:

: 128350-30-1,128441-43-0
C₂₃H₂₆N₂

: 139750-89-3
(1RS,5RS,12SR)-benzyl 12-ethyl-6-oxo-1,2,3,4,5,6-hexahydro-1,5-methanoazocino[4,3-b]indole-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / Pd(OH)2 / methanol

2: K₂CO₃ / CH₂Cl₂

3: 43 percent / SeO₂ / dioxane / 40 h / 80 °C

With selenium(IV) oxide; hydrogen; potassium carbonate; palladium dihydroxide; In 1,4-dioxane; methanol; dichloromethane;
DOI:10.1039/c39910001687