trans-5--15-phenyl>-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin

Base Information

• Chemical Name: trans-5--15-phenyl>-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin
• CAS No.: 94111-77-0
• Molecular Formula: C₆₄H₇₅N₇O₄
• Molecular Weight: 1006.34

Synonyms:trans-5--15-phenyl>-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin

Chemical Property of trans-5--15-phenyl>-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin

Chemical Property:

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Technology Process of trans-5--15-phenyl>-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin

There total 1 articles about trans-5--15-phenyl>-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(tert-butoxycarbonyl)-4-aminobutanoic acid (57294-38-9) + 4-tert-Butyl-N-{2-[(5Z,10Z,14Z,19Z)-15-(2-tert-butylamino-phenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethyl-porphyrin-5-yl]-phenyl}-benzamide → trans-5--15-phenyl>-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin (94111-77-0)

Guidance literature:

With chloroformic acid ethyl ester; triethylamine; Multistep reaction; 1.) toluene; 2.) THF, toluene, 3 h, reflux;

DOI:10.1021/ja00290a027

Reference yield:

trans-5--15-phenyl>-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin (94111-77-0) → trans-5--15--2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin (94111-78-1)

Guidance literature:

With hydrogenchloride; In acetic acid; for 0.166667h; Ambient temperature;

DOI:10.1021/ja00290a027

upstream raw materials:

N-(tert-butoxycarbonyl)-4-aminobutanoic acid

Downstream raw materials:

trans-5--15--2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin

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