Trifluoro-acetic acid 9-tert-butyl-2,2,6,6-tetrakis-trifluoromethyl-4-(2,2,2-trifluoro-1-phenyl-1-trifluoromethyl-ethoxy)-4λ⁵-ioda-3,5-dioxa-tricyclo[5.3.1.0^4,11]undeca-1(10),7(11),8-trien-4-yl ester

Base Information

• Chemical Name: Trifluoro-acetic acid 9-tert-butyl-2,2,6,6-tetrakis-trifluoromethyl-4-(2,2,2-trifluoro-1-phenyl-1-trifluoromethyl-ethoxy)-4λ⁵-ioda-3,5-dioxa-tricyclo[5.3.1.0^4,11]undeca-1(10),7(11),8-trien-4-yl ester
• CAS No.: 136213-59-7
• Molecular Formula: C₂₇H₁₆F₂₁IO₅
• Molecular Weight: 946.292

Synonyms:Trifluoro-acetic acid 9-tert-butyl-2,2,6,6-tetrakis-trifluoromethyl-4-(2,2,2-trifluoro-1-phenyl-1-trifluoromethyl-ethoxy)-4λ⁵-ioda-3,5-dioxa-tricyclo[5.3.1.0^4,11]undeca-1(10),7(11),8-trien-4-yl ester

Chemical Property of Trifluoro-acetic acid 9-tert-butyl-2,2,6,6-tetrakis-trifluoromethyl-4-(2,2,2-trifluoro-1-phenyl-1-trifluoromethyl-ethoxy)-4λ⁵-ioda-3,5-dioxa-tricyclo[5.3.1.0^4,11]undeca-1(10),7(11),8-trien-4-yl ester

Chemical Property:

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Technology Process of Trifluoro-acetic acid 9-tert-butyl-2,2,6,6-tetrakis-trifluoromethyl-4-(2,2,2-trifluoro-1-phenyl-1-trifluoromethyl-ethoxy)-4λ⁵-ioda-3,5-dioxa-tricyclo[5.3.1.0^4,11]undeca-1(10),7(11),8-trien-4-yl ester

There total 2 articles about Trifluoro-acetic acid 9-tert-butyl-2,2,6,6-tetrakis-trifluoromethyl-4-(2,2,2-trifluoro-1-phenyl-1-trifluoromethyl-ethoxy)-4λ⁵-ioda-3,5-dioxa-tricyclo[5.3.1.0^4,11]undeca-1(10),7(11),8-trien-4-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Martins sulfurane (32133-82-7) → Trifluoro-acetic acid 9-tert-butyl-2,2,6,6-tetrakis-trifluoromethyl-4-(2,2,2-trifluoro-1-phenyl-1-trifluoromethyl-ethoxy)-4λ5-ioda-3,5-dioxa-tricyclo[5.3.1.04,11]undeca-1(10),7(11),8-trien-4-yl ester (136213-59-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / CH₂Cl₂ / 0.25 h / Ambient temperature

2: 25 percent Spectr_. / 4 h / Ambient temperature

In dichloromethane;

DOI:10.1021/jo00023a022

Reference yield:

1,1-bis<1-phenyl-1-(trifluoromethyl)-2,2,2-trifluoroethoxy>-10-tert-butyl-3,3,7,7-tetrakis(trifluoromethyl)-4,6-benzo-1-ioda-2,8-dioxabicyclo<3.3.0>octane (136213-56-4) + trifluoroacetic anhydride (407-25-0) → 1,1-bis(trifloroacetoxy)-10-tert-butyl-3,3,7,7-tetrakis(trifluoromethyl)-4,6-benzo-1-ioda-2,8-dioxabicyclo<3.3.0>octane (136213-53-1) + Trifluoro-acetic acid 9-tert-butyl-2,2,6,6-tetrakis-trifluoromethyl-4-(2,2,2-trifluoro-1-phenyl-1-trifluoromethyl-ethoxy)-4λ5-ioda-3,5-dioxa-tricyclo[5.3.1.04,11]undeca-1(10),7(11),8-trien-4-yl ester (136213-59-7)

Guidance literature:

for 4h; Ambient temperature;

DOI:10.1021/jo00023a022

upstream raw materials:

1,1-bis<1-phenyl-1-(trifluoromethyl)-2,2,2-trifluoroethoxy>-10-tert-butyl-3,3,7,7-tetrakis(trifluoromethyl)-4,6-benzo-1-ioda-2,8-dioxabicyclo<3.3.0>octane

trifluoroacetic anhydride

Martins sulfurane

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