oleanate 28-O-6-phthalimido-6-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:oleanate 28-O-6-phthalimido-6-deoxy-β-D-glucopyranoside
CAS No.:1609984-10-2
Molecular Formula:C₄₄H₆₃NO₁₀
Molecular Weight:765.985
Hs Code.:

Synonyms:oleanate 28-O-6-phthalimido-6-deoxy-β-D-glucopyranoside

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Chemical Property of oleanate 28-O-6-phthalimido-6-deoxy-β-D-glucopyranoside

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Technology Process of oleanate 28-O-6-phthalimido-6-deoxy-β-D-glucopyranoside

There total 7 articles about oleanate 28-O-6-phthalimido-6-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₆₅H₇₅NO₁₃

: 1609984-10-2
oleanate 28-O-6-phthalimido-6-deoxy-β-D-glucopyranoside

Guidance literature:: With sodium methylate; In methanol; dichloromethane; at 20 ℃; for 9h;
DOI:10.1016/j.ejmech.2014.03.080

Reference yield:

: 104707-01-9
1,2,3,4-tetra-O-benzoyl-β-D-glucopyranose

: 1609984-10-2
oleanate 28-O-6-phthalimido-6-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 7 steps

1.1: p-toluenesulfonyl chloride; pyridine; dmap / 20 h / 20 °C

1.2: 24 h / 60 °C

2.1: trimethylphosphane / tetrahydrofuran / 120 h / 20 °C

3.1: potassium carbonate / tetrahydrofuran / 5 h / 60 °C

4.1: acetic acid; hydrogen bromide / dichloromethane / 6 h / 20 °C

5.1: potassium carbonate; tetrabutylammomium bromide / dichloromethane; water / 6 h / Reflux

6.1: palladium 10% on activated carbon; hydrogen / methanol; dichloromethane / 5 h / 760.05 Torr

7.1: sodium methylate / methanol; dichloromethane / 9 h / 20 °C

With pyridine; dmap; palladium 10% on activated carbon; tetrabutylammomium bromide; hydrogen bromide; hydrogen; sodium methylate; potassium carbonate; acetic acid; p-toluenesulfonyl chloride; trimethylphosphane; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1016/j.ejmech.2014.03.080

Reference yield:

: 1609983-69-8
6-azide-1,2,3,4-tetra-O-benzoyl-6-deoxy-β-D-glucopyranose

: 1609984-10-2
oleanate 28-O-6-phthalimido-6-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: trimethylphosphane / tetrahydrofuran / 120 h / 20 °C

2: potassium carbonate / tetrahydrofuran / 5 h / 60 °C

3: acetic acid; hydrogen bromide / dichloromethane / 6 h / 20 °C

4: potassium carbonate; tetrabutylammomium bromide / dichloromethane; water / 6 h / Reflux

5: palladium 10% on activated carbon; hydrogen / methanol; dichloromethane / 5 h / 760.05 Torr

6: sodium methylate / methanol; dichloromethane / 9 h / 20 °C

With palladium 10% on activated carbon; tetrabutylammomium bromide; hydrogen bromide; hydrogen; sodium methylate; potassium carbonate; acetic acid; trimethylphosphane; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1016/j.ejmech.2014.03.080