2-(benzyloxymethyl)-3,3-dimethylbutyl toluene-p-sulfonate

Base Information

Chemical Name:2-(benzyloxymethyl)-3,3-dimethylbutyl toluene-p-sulfonate
CAS No.:201985-35-5
Molecular Formula:C₂₁H₂₈O₄S
Molecular Weight:376.517
Hs Code.:

Synonyms:2-(benzyloxymethyl)-3,3-dimethylbutyl toluene-p-sulfonate

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Chemical Property of 2-(benzyloxymethyl)-3,3-dimethylbutyl toluene-p-sulfonate

Chemical Property:

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Technology Process of 2-(benzyloxymethyl)-3,3-dimethylbutyl toluene-p-sulfonate

There total 4 articles about 2-(benzyloxymethyl)-3,3-dimethylbutyl toluene-p-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 98-59-9
p-toluenesulfonyl chloride

: 138741-39-6
2-<(benzyloxy)methyl>-3,3-dimethylbutan-1-ol

: 201985-35-5
2-(benzyloxymethyl)-3,3-dimethylbutyl toluene-p-sulfonate

Guidance literature:: With dmap; In pyridine; dichloromethane; for 12h; Ambient temperature;
DOI:10.1039/a608488e

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 201985-35-5
2-(benzyloxymethyl)-3,3-dimethylbutyl toluene-p-sulfonate

Guidance literature:: Multi-step reaction with 3 steps

2: 90 percent / LiAlH₄ / tetrahydrofuran / 1.) reflux, 10 min, 2.) room temperature, overnight

3: 98 percent / 4-(N,N-dimethylamino)pyridine / pyridine; CH₂Cl₂ / 12 h / Ambient temperature

With dmap; lithium aluminium tetrahydride; In tetrahydrofuran; pyridine; dichloromethane;
DOI:10.1039/a608488e

Reference yield:

: 1070-83-3
tert-Butylacetic acid

: 201985-35-5
2-(benzyloxymethyl)-3,3-dimethylbutyl toluene-p-sulfonate

Guidance literature:: Multi-step reaction with 3 steps

2: 90 percent / LiAlH₄ / tetrahydrofuran / 1.) reflux, 10 min, 2.) room temperature, overnight

3: 98 percent / 4-(N,N-dimethylamino)pyridine / pyridine; CH₂Cl₂ / 12 h / Ambient temperature

With dmap; lithium aluminium tetrahydride; In tetrahydrofuran; pyridine; dichloromethane;
DOI:10.1039/a608488e