benzyl 4-O-benzoyl-2-bromo-3-O-(2-bromo-2,6-dideoxy-β-D-glucopyranosyl)-2,6-dideoxy-β-D-glucopyranoside

Base Information

• Chemical Name: benzyl 4-O-benzoyl-2-bromo-3-O-(2-bromo-2,6-dideoxy-β-D-glucopyranosyl)-2,6-dideoxy-β-D-glucopyranoside
• CAS No.: 94820-95-8
• Molecular Formula: C₂₆H₃₀Br₂O₈
• Molecular Weight: 630.327
• Mol file: 94820-95-8.mol

Synonyms:benzyl 4-O-benzoyl-2-bromo-3-O-(2-bromo-2,6-dideoxy-β-D-glucopyranosyl)-2,6-dideoxy-β-D-glucopyranoside

Chemical Property of benzyl 4-O-benzoyl-2-bromo-3-O-(2-bromo-2,6-dideoxy-β-D-glucopyranosyl)-2,6-dideoxy-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of benzyl 4-O-benzoyl-2-bromo-3-O-(2-bromo-2,6-dideoxy-β-D-glucopyranosyl)-2,6-dideoxy-β-D-glucopyranoside

There total 1 articles about benzyl 4-O-benzoyl-2-bromo-3-O-(2-bromo-2,6-dideoxy-β-D-glucopyranosyl)-2,6-dideoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

C34H34Br2O10 (86448-03-5) → benzyl 4-O-benzoyl-2-bromo-3-O-(2-bromo-2,6-dideoxy-β-D-glucopyranosyl)-2,6-dideoxy-β-D-glucopyranoside (94820-95-8)

Guidance literature:

With sodium methylate; In methanol; for 5h; Ambient temperature;

DOI:10.1021/jo00207a009

Reference yield: 97.0%

acetic anhydride (108-24-7) + benzyl 4-O-benzoyl-2-bromo-3-O-(2-bromo-2,6-dideoxy-β-D-glucopyranosyl)-2,6-dideoxy-β-D-glucopyranoside (94820-95-8) → benzyl 3-O-(3,4-di-O-acetyl-2-bromo-2,6-dideoxy-β-D-glucopyranosyl)-4-O-benzoyl-2-bromo-2,6-dideoxy-β-D-glucopyranoside (94820-96-9)

Guidance literature:

With pyridine; at 5 ℃; for 24h;

DOI:10.1021/jo00207a009

Reference yield: 46.0%

benzyl 4-O-benzoyl-2-bromo-3-O-(2-bromo-2,6-dideoxy-β-D-glucopyranosyl)-2,6-dideoxy-β-D-glucopyranoside (94820-95-8) → benzyl-4-O-benzoyl-3-O-(2,6-dideoxy-β-D-erythro-hexopyranos-3-ulosyl)-2,6-dideoxy-β-D-arabino-hexopyranoside (94821-00-8) + benzyl-4-O-benzoyl-3-O-(2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranoside (94820-99-2)

Guidance literature:

With hydrogen; triethylamine; palladium on activated charcoal; In ethyl acetate; for 24h; Ambient temperature;

DOI:10.1021/jo00207a009

upstream raw materials:

C₃₄H₃₄Br₂O₁₀

Downstream raw materials:

benzyl 3-O-(3,4-di-O-acetyl-2-bromo-2,6-dideoxy-β-D-glucopyranosyl)-4-O-benzoyl-2-bromo-2,6-dideoxy-β-D-glucopyranoside

benzyl-4-O-benzoyl-3-O-(2,6-dideoxy-β-D-erythro-hexopyranos-3-ulosyl)-2,6-dideoxy-β-D-arabino-hexopyranoside

benzyl-4-O-benzoyl-3-O-(2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranoside

benzyl 3-O-(4-O-acetyl-2,6-dideoxy-β-D-erythro-hexopyranos-3-ulosyl)-4-O-benzoyl-2,6-dideoxy-β-D-arabino-hexopyranoside