Technology Process of 1-(4-(4-aminophenoxy)phenyl)-1-(4-aminophenyl)-1-(6-oxido-6H-dibenz[c,e][1,2]oxaphosphorin-6-yl)ethane
There total 6 articles about 1-(4-(4-aminophenoxy)phenyl)-1-(4-aminophenyl)-1-(6-oxido-6H-dibenz[c,e][1,2]oxaphosphorin-6-yl)ethane which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 24h;
under 7240.26 Torr;
Autoclave;
DOI:10.1002/pola.24552
- Guidance literature:
-
Multi-step reaction with 3 steps
1: toluene-4-sulfonic acid / 24 h / 130 °C / Inert atmosphere
2: potassium carbonate / N,N-dimethyl acetamide / 12 h / 120 °C / Inert atmosphere
3: palladium 10% on activated carbon; hydrogen / N,N-dimethyl-formamide / 24 h / 20 °C / 7240.26 Torr / Autoclave
With
palladium 10% on activated carbon; hydrogen; potassium carbonate; toluene-4-sulfonic acid;
In
N,N-dimethyl acetamide; N,N-dimethyl-formamide;
DOI:10.1002/pola.24552
- Guidance literature:
-
Multi-step reaction with 3 steps
1: toluene-4-sulfonic acid / 24 h / 130 °C / Inert atmosphere
2: potassium carbonate / N,N-dimethyl acetamide / 12 h / 120 °C / Inert atmosphere
3: palladium 10% on activated carbon; hydrogen / N,N-dimethyl-formamide / 24 h / 20 °C / 7240.26 Torr / Autoclave
With
palladium 10% on activated carbon; hydrogen; potassium carbonate; toluene-4-sulfonic acid;
In
N,N-dimethyl acetamide; N,N-dimethyl-formamide;
DOI:10.1002/pola.24552
