1-(4-(4-aminophenoxy)phenyl)-1-(4-aminophenyl)-1-(6-oxido-6H-dibenz[c,e][1,2]oxaphosphorin-6-yl)ethane

Base Information

Chemical Name:1-(4-(4-aminophenoxy)phenyl)-1-(4-aminophenyl)-1-(6-oxido-6H-dibenz[c,e][1,2]oxaphosphorin-6-yl)ethane
CAS No.:1268247-25-1
Molecular Formula:C₃₂H₂₇N₂O₃P
Molecular Weight:518.552
Hs Code.:

Synonyms:1-(4-(4-aminophenoxy)phenyl)-1-(4-aminophenyl)-1-(6-oxido-6H-dibenz[c,e][1,2]oxaphosphorin-6-yl)ethane

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Chemical Property of 1-(4-(4-aminophenoxy)phenyl)-1-(4-aminophenyl)-1-(6-oxido-6H-dibenz[c,e][1,2]oxaphosphorin-6-yl)ethane

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Technology Process of 1-(4-(4-aminophenoxy)phenyl)-1-(4-aminophenyl)-1-(6-oxido-6H-dibenz[c,e][1,2]oxaphosphorin-6-yl)ethane

There total 6 articles about 1-(4-(4-aminophenoxy)phenyl)-1-(4-aminophenyl)-1-(6-oxido-6H-dibenz[c,e][1,2]oxaphosphorin-6-yl)ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1268247-24-0
C₃₂H₂₅N₂O₅P

: 1268247-25-1
1-(4-(4-aminophenoxy)phenyl)-1-(4-aminophenyl)-1-(6-oxido-6H-dibenz[c,e][1,2]oxaphosphorin-6-yl)ethane

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In N,N-dimethyl-formamide; at 20 ℃; for 24h; under 7240.26 Torr; Autoclave;
DOI:10.1002/pola.24552

Reference yield:

: 62-53-3
aniline

: 1268247-25-1
1-(4-(4-aminophenoxy)phenyl)-1-(4-aminophenyl)-1-(6-oxido-6H-dibenz[c,e][1,2]oxaphosphorin-6-yl)ethane

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / 24 h / 130 °C / Inert atmosphere

2: potassium carbonate / N,N-dimethyl acetamide / 12 h / 120 °C / Inert atmosphere

3: palladium 10% on activated carbon; hydrogen / N,N-dimethyl-formamide / 24 h / 20 °C / 7240.26 Torr / Autoclave

With palladium 10% on activated carbon; hydrogen; potassium carbonate; toluene-4-sulfonic acid; In N,N-dimethyl acetamide; N,N-dimethyl-formamide;
DOI:10.1002/pola.24552

Reference yield:

: 99-93-4
4-Hydroxyacetophenone

: 1268247-25-1
1-(4-(4-aminophenoxy)phenyl)-1-(4-aminophenyl)-1-(6-oxido-6H-dibenz[c,e][1,2]oxaphosphorin-6-yl)ethane

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / 24 h / 130 °C / Inert atmosphere

2: potassium carbonate / N,N-dimethyl acetamide / 12 h / 120 °C / Inert atmosphere

3: palladium 10% on activated carbon; hydrogen / N,N-dimethyl-formamide / 24 h / 20 °C / 7240.26 Torr / Autoclave

With palladium 10% on activated carbon; hydrogen; potassium carbonate; toluene-4-sulfonic acid; In N,N-dimethyl acetamide; N,N-dimethyl-formamide;
DOI:10.1002/pola.24552