(R,S)-N-(tert-butyloxycarbonyl)-L-tyrosyl-D-methionylglycine 1,3-dimethylbutyl amide

Base Information

Chemical Name:(R,S)-N-(tert-butyloxycarbonyl)-L-tyrosyl-D-methionylglycine 1,3-dimethylbutyl amide
CAS No.:78537-10-7
Molecular Formula:C₂₇H₄₄N₄O₆S
Molecular Weight:552.736
Hs Code.:

Synonyms:(R,S)-N-(tert-butyloxycarbonyl)-L-tyrosyl-D-methionylglycine 1,3-dimethylbutyl amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R,S)-N-(tert-butyloxycarbonyl)-L-tyrosyl-D-methionylglycine 1,3-dimethylbutyl amide

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Technology Process of (R,S)-N-(tert-butyloxycarbonyl)-L-tyrosyl-D-methionylglycine 1,3-dimethylbutyl amide

There total 2 articles about (R,S)-N-(tert-butyloxycarbonyl)-L-tyrosyl-D-methionylglycine 1,3-dimethylbutyl amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 15761-50-9,34017-11-3,54548-48-0,108-09-8
2-amino-4-methylpentane

: 70777-31-0
N-(tert-butyloxycarbonyl)-L-tyrosyl-D-methionylglycine methyl ester

: 78537-10-7
(R,S)-N-(tert-butyloxycarbonyl)-L-tyrosyl-D-methionylglycine 1,3-dimethylbutyl amide

Guidance literature:: In methanol; for 192h; Ambient temperature;
DOI:10.1021/jm00142a002

Reference yield:

: 3978-80-1
Boc-Tyr-OH

: 78537-10-7
(R,S)-N-(tert-butyloxycarbonyl)-L-tyrosyl-D-methionylglycine 1,3-dimethylbutyl amide

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / triethylamine, 1-hydroxybenzotriazole (HOBT), dicyclohexylcarbodiimide (DCC) / tetrahydrofuran; CHCl₃ / 1.) 0 deg C, 1 h, 2.) RT, overnight

2: 90 percent / methanol / 192 h / Ambient temperature

With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; chloroform;
DOI:10.1021/jm00142a002