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C35H61NO5

Base Information
  • Chemical Name:C35H61NO5
  • CAS No.:1454597-79-5
  • Molecular Formula:C35H61NO5
  • Molecular Weight:575.873
  • Hs Code.:
C<sub>35</sub>H<sub>61</sub>NO<sub>5</sub>

Synonyms:C35H61NO5

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Chemical Property of C35H61NO5
Chemical Property:
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Technology Process of C35H61NO5

There total 21 articles about C35H61NO5 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With [Ir(cod)(SIMes)(Pyr)]+PF6-; hydrogen; In dichloromethane; at 20 ℃; for 18h; under 67506.8 Torr; diastereoselective reaction; Autoclave;
DOI:10.1002/anie.201303776
Guidance literature:
Multi-step reaction with 7 steps
1.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere
2.1: water; sodium hydroxide / methanol / 1 h / Reflux
3.1: methyllithium / tetrahydrofuran / 0.67 h / -20 - 20 °C / Inert atmosphere
3.2: 1 h / 40 °C / Inert atmosphere
3.3: 0.25 h / 0 °C / Inert atmosphere
4.1: tert.-butyl lithium / diethyl ether; pentane / 0.17 h / -78 °C / Inert atmosphere
4.2: 2 h / -78 - 20 °C / Inert atmosphere
4.3: 2 h / 20 °C / Darkness
5.1: pyridine / dichloromethane / 1 h / 0 °C / Inert atmosphere
6.1: tetra-N-butylammonium tribromide / methanol / 4 h / 20 °C / Inert atmosphere
7.1: hydrogen; [Ir(cod)(SIMes)(Pyr)]+PF6- / dichloromethane / 18 h / 20 °C / 67506.8 Torr / Autoclave
With pyridine; di-isopropyl azodicarboxylate; [Ir(cod)(SIMes)(Pyr)]+PF6-; water; methyllithium; hydrogen; tert.-butyl lithium; tetra-N-butylammonium tribromide; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; pentane;
DOI:10.1002/anie.201303776
Guidance literature:
Multi-step reaction with 5 steps
1.1: triphenylphosphine; iodine; 1H-imidazole / acetonitrile; diethyl ether / 0.5 h / 0 °C / Inert atmosphere
2.1: tert.-butyl lithium / diethyl ether; pentane / 0.17 h / -78 °C / Inert atmosphere
2.2: 2 h / -78 - 20 °C / Inert atmosphere
2.3: 2 h / 20 °C / Darkness
3.1: pyridine / dichloromethane / 1 h / 0 °C / Inert atmosphere
4.1: tetra-N-butylammonium tribromide / methanol / 4 h / 20 °C / Inert atmosphere
5.1: hydrogen; [Ir(cod)(SIMes)(Pyr)]+PF6- / dichloromethane / 18 h / 20 °C / 67506.8 Torr / Autoclave
With pyridine; 1H-imidazole; [Ir(cod)(SIMes)(Pyr)]+PF6-; hydrogen; iodine; tert.-butyl lithium; tetra-N-butylammonium tribromide; triphenylphosphine; In methanol; diethyl ether; dichloromethane; acetonitrile; pentane;
DOI:10.1002/anie.201303776
upstream raw materials:

C18H35IO

octadec-1-yn-3-ol

C16H36O2Si

C16H35IOSi

Downstream raw materials:

C50H90O2Si2

C44H76O2Si

C44H75IOSi

C41H75NO5Si

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