2-(1H-Indol-3-yl)ethyl 2,3,4-Tri-O-benzyl-6-O-(5-aminopentyl)-β-D-glucopyranoside

Base Information

Chemical Name:2-(1H-Indol-3-yl)ethyl 2,3,4-Tri-O-benzyl-6-O-(5-aminopentyl)-β-D-glucopyranoside
CAS No.:132132-78-6
Molecular Formula:C₄₂H₅₀N₂O₆
Molecular Weight:678.869
Hs Code.:

Synonyms:2-(1H-Indol-3-yl)ethyl 2,3,4-Tri-O-benzyl-6-O-(5-aminopentyl)-β-D-glucopyranoside

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Chemical Property of 2-(1H-Indol-3-yl)ethyl 2,3,4-Tri-O-benzyl-6-O-(5-aminopentyl)-β-D-glucopyranoside

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Technology Process of 2-(1H-Indol-3-yl)ethyl 2,3,4-Tri-O-benzyl-6-O-(5-aminopentyl)-β-D-glucopyranoside

There total 14 articles about 2-(1H-Indol-3-yl)ethyl 2,3,4-Tri-O-benzyl-6-O-(5-aminopentyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 132132-78-6
2-(1H-Indol-3-yl)ethyl 2,3,4-Tri-O-benzyl-6-O-(5-aminopentyl)-β-D-glucopyranoside

Guidance literature:

Reference yield: 91.0%

: 170219-83-7
2-(1-phenylsulfonyl-indol-3yl)ethyl-6-O-(5-aminopentyl)-2,3,4-tri-O-benzyl-β-D-glucopyranoside

: 132132-78-6
2-(1H-Indol-3-yl)ethyl 2,3,4-Tri-O-benzyl-6-O-(5-aminopentyl)-β-D-glucopyranoside

Guidance literature:: With sodium hydroxide; In ethanol; for 3h; Heating;

Reference yield:

: 526-55-6,930395-07-6
2-(3-indole)-ethanol

: 132132-78-6
2-(1H-Indol-3-yl)ethyl 2,3,4-Tri-O-benzyl-6-O-(5-aminopentyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 11 steps

1: 99 percent / imidazole / dimethylformamide / 16 h / Ambient temperature

2: 1.) NaH / 1.) DMF, RT, 30 min, 2.) DMF, RT, 16 h

3: 84 percent / tetrabutylammonium fluoride / tetrahydrofuran / 16 h / Ambient temperature

4: 64 percent / Ag₂O, 4A molecular sieves / benzene; hexane / 96 h / Ambient temperature

5: 88 percent / NaOMe / methanol / 0.33 h / Ambient temperature

6: 85 percent / imidazole / dimethylformamide / 24 h / 50 °C

7: 1.) NaH, 2.) tetrabutylammonium iodide / 1.) THF, RT, 1 h, 2.) THF, RT, 3 d

8: 94 percent / tetrabutylammonium fluoride / tetrahydrofuran / 7 h / Ambient temperature

9: NaH / CH₂Cl₂ / 24 h / Ambient temperature

10: 86 percent / triphenylphosphine / tetrahydrofuran; H₂O / 2.5 h / Heating

11: 91 percent / 5 M aq. NaOH / ethanol / 3 h / Heating

With 1H-imidazole; sodium hydroxide; 4 A molecular sieve; tetrabutyl ammonium fluoride; sodium methylate; tetra-(n-butyl)ammonium iodide; sodium hydride; triphenylphosphine; silver(l) oxide; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; benzene;