4-[(5-benzyloxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-methoxymethoxy-methyl]-2,2-dimethyl-[1,3]dioxan-5-one

Base Information

• Chemical Name: 4-[(5-benzyloxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-methoxymethoxy-methyl]-2,2-dimethyl-[1,3]dioxan-5-one
• CAS No.: 929207-23-8
• Molecular Formula: C₂₂H₃₂O₈
• Molecular Weight: 424.491

Synonyms:4-[(5-benzyloxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-methoxymethoxy-methyl]-2,2-dimethyl-[1,3]dioxan-5-one

Chemical Property of 4-[(5-benzyloxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-methoxymethoxy-methyl]-2,2-dimethyl-[1,3]dioxan-5-one

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Technology Process of 4-[(5-benzyloxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-methoxymethoxy-methyl]-2,2-dimethyl-[1,3]dioxan-5-one

There total 3 articles about 4-[(5-benzyloxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-methoxymethoxy-methyl]-2,2-dimethyl-[1,3]dioxan-5-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

4-[(5-benzyloxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-hydroxy-methyl]-2,2-dimethyl-[1,3]dioxan-5-one (929207-21-6) + chloromethyl methyl ether (107-30-2) → 4-[(5-benzyloxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-methoxymethoxy-methyl]-2,2-dimethyl-[1,3]dioxan-5-one (929207-23-8)

Guidance literature:

With 2,6-dimethylpyridine; tertamethylammonium iodide; In dichloromethane; at 20 ℃;

DOI:10.1055/s-2006-956495

Reference yield:

2,2,-dimethyl-1,3-dioxan-5-one (74181-34-3) → 4-[(5-benzyloxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-methoxymethoxy-methyl]-2,2-dimethyl-[1,3]dioxan-5-one (929207-23-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 69 percent / (R)-proline / dimethylformamide / 20 °C

2: 99 percent / 2,6-lutidine; Me₄NI / CH₂Cl₂ / 20 °C

With 2,6-dimethylpyridine; tertamethylammonium iodide; D-Prolin; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1055/s-2006-956495

Reference yield:

4-O-benzyl-2,3-O-isopropylidene-D-threose (81801-09-4) → 4-[(5-benzyloxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-methoxymethoxy-methyl]-2,2-dimethyl-[1,3]dioxan-5-one (929207-23-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 69 percent / (R)-proline / dimethylformamide / 20 °C

2: 99 percent / 2,6-lutidine; Me₄NI / CH₂Cl₂ / 20 °C

With 2,6-dimethylpyridine; tertamethylammonium iodide; D-Prolin; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1055/s-2006-956495

upstream raw materials:

4-[(5-benzyloxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-hydroxy-methyl]-2,2-dimethyl-[1,3]dioxan-5-one

chloromethyl methyl ether

2,2,-dimethyl-1,3-dioxan-5-one

4-O-benzyl-2,3-O-isopropylidene-D-threose

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