N-[3-(3-(3-trifluoromethyl)-benzoylaminophenyldisulfanyl)-phenyl]-benzamide

Base Information

Chemical Name:N-[3-(3-(3-trifluoromethyl)-benzoylaminophenyldisulfanyl)-phenyl]-benzamide
CAS No.:1616689-88-3
Molecular Formula:C₂₈H₁₈F₆N₂O₂S₂
Molecular Weight:592.586
Hs Code.:

Synonyms:N-[3-(3-(3-trifluoromethyl)-benzoylaminophenyldisulfanyl)-phenyl]-benzamide

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Chemical Property of N-[3-(3-(3-trifluoromethyl)-benzoylaminophenyldisulfanyl)-phenyl]-benzamide

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Technology Process of N-[3-(3-(3-trifluoromethyl)-benzoylaminophenyldisulfanyl)-phenyl]-benzamide

There total 2 articles about N-[3-(3-(3-trifluoromethyl)-benzoylaminophenyldisulfanyl)-phenyl]-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 454-92-2
3-(trifluoromethyl)benzoic acid

: 40897-41-4
bis(3-aminophenyl)-disulfide

: 1616689-88-3
N-[3-(3-(3-trifluoromethyl)-benzoylaminophenyldisulfanyl)-phenyl]-benzamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 20 - 60 ℃;

Reference yield:

: 22948-02-3
3-aminothiophenol

: 1616689-88-3
N-[3-(3-(3-trifluoromethyl)-benzoylaminophenyldisulfanyl)-phenyl]-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: dimethyl sulfoxide / 4 h / 90 °C

2: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 20 - 60 °C

With N-ethyl-N,N-diisopropylamine; HATU; In dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield: 8.0%

: 1616689-88-3
N-[3-(3-(3-trifluoromethyl)-benzoylaminophenyldisulfanyl)-phenyl]-benzamide

: 1616689-89-4
5-bromomethyl-1H-pyrrolo[2,3-b]pyridine-2-carboxylic acid methyl ester

: 1616689-52-1
5-[3-(3-trifluoromethylbenzoylamino)-phenylsulfanylmethyl]-1H-pyrrolo[2,3-b]pyridine-2-carboxylic acid methyl ester

Guidance literature:: N-[3-(3-(3-trifluoromethyl)-benzoylaminophenyldisulfanyl)-phenyl]-benzamide; With triphenylphosphine; In acetonitrile; at 20 ℃;

5-bromomethyl-1H-pyrrolo[2,3-b]pyridine-2-carboxylic acid methyl ester; With potassium carbonate; sodium iodide; In acetonitrile; for 6h; Reflux;