N-(1-{4-[(hydroxyamino)carbonyl]phenyl}ethyl)-1-methyl-1H-pyrrole-2-carboxamide

Base Information

Chemical Name:N-(1-{4-[(hydroxyamino)carbonyl]phenyl}ethyl)-1-methyl-1H-pyrrole-2-carboxamide
CAS No.:1332892-85-9
Molecular Formula:C₁₅H₁₇N₃O₃
Molecular Weight:287.318
Hs Code.:

Synonyms:N-(1-{4-[(hydroxyamino)carbonyl]phenyl}ethyl)-1-methyl-1H-pyrrole-2-carboxamide

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Chemical Property of N-(1-{4-[(hydroxyamino)carbonyl]phenyl}ethyl)-1-methyl-1H-pyrrole-2-carboxamide

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Technology Process of N-(1-{4-[(hydroxyamino)carbonyl]phenyl}ethyl)-1-methyl-1H-pyrrole-2-carboxamide

There total 4 articles about N-(1-{4-[(hydroxyamino)carbonyl]phenyl}ethyl)-1-methyl-1H-pyrrole-2-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₁₈N₂O₃

: 1332892-85-9
N-(1-{4-[(hydroxyamino)carbonyl]phenyl}ethyl)-1-methyl-1H-pyrrole-2-carboxamide

Guidance literature:: C₁₆H₁₈N₂O₃; With hydroxylamine hydrochloride; potassium hydroxide; In methanol; at 20 - 80 ℃; for 5.5h;

With formic acid; In methanol;

Reference yield:

: 74733-31-6
methyl 4-(1-(hydroxyimino)ethyl)benzoate

: 1332892-85-9
N-(1-{4-[(hydroxyamino)carbonyl]phenyl}ethyl)-1-methyl-1H-pyrrole-2-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / palladium 10% on activated carbon / water; methanol / 20 °C

2: 4-methyl-morpholine; HATU / dichloromethane / 20 °C

3: hydroxylamine hydrochloride; potassium hydroxide / methanol / 5.5 h / 20 - 80 °C

With 4-methyl-morpholine; hydrogenchloride; hydroxylamine hydrochloride; HATU; potassium hydroxide; palladium 10% on activated carbon; In methanol; dichloromethane; water;

Reference yield:

: 3609-53-8
methyl 4-acetylbenzoate

: 1332892-85-9
N-(1-{4-[(hydroxyamino)carbonyl]phenyl}ethyl)-1-methyl-1H-pyrrole-2-carboxamide

Guidance literature:: Multi-step reaction with 4 steps

1: hydroxylamine hydrochloride; sodium acetate / methanol / 2 h / 40 °C

2: hydrogenchloride / palladium 10% on activated carbon / water; methanol / 20 °C

3: 4-methyl-morpholine; HATU / dichloromethane / 20 °C

4: hydroxylamine hydrochloride; potassium hydroxide / methanol / 5.5 h / 20 - 80 °C

With 4-methyl-morpholine; hydrogenchloride; hydroxylamine hydrochloride; sodium acetate; HATU; potassium hydroxide; palladium 10% on activated carbon; In methanol; dichloromethane; water;