[2-(4-chloro-2-methoxyphenyl)-4-methylthiazol-5-yl]carbamic acid 1,2,3,4-tetrahydrobenzo[4,5]imidazo[1,2-a]pyridin-7-ylmethyl ester

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Chemical Name:[2-(4-chloro-2-methoxyphenyl)-4-methylthiazol-5-yl]carbamic acid 1,2,3,4-tetrahydrobenzo[4,5]imidazo[1,2-a]pyridin-7-ylmethyl ester
CAS No.:1354397-05-9
Molecular Formula:C₂₄H₂₃ClN₄O₃S
Molecular Weight:482.991
Hs Code.:

Synonyms:[2-(4-chloro-2-methoxyphenyl)-4-methylthiazol-5-yl]carbamic acid 1,2,3,4-tetrahydrobenzo[4,5]imidazo[1,2-a]pyridin-7-ylmethyl ester

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Chemical Property of [2-(4-chloro-2-methoxyphenyl)-4-methylthiazol-5-yl]carbamic acid 1,2,3,4-tetrahydrobenzo[4,5]imidazo[1,2-a]pyridin-7-ylmethyl ester

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Technology Process of [2-(4-chloro-2-methoxyphenyl)-4-methylthiazol-5-yl]carbamic acid 1,2,3,4-tetrahydrobenzo[4,5]imidazo[1,2-a]pyridin-7-ylmethyl ester

There total 10 articles about [2-(4-chloro-2-methoxyphenyl)-4-methylthiazol-5-yl]carbamic acid 1,2,3,4-tetrahydrobenzo[4,5]imidazo[1,2-a]pyridin-7-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1354406-86-2
(1,2,3,4-tetrahydrobenzo[4,5]imidazo[1,2-a]pyridine-7-yl)methanol

: 1354407-32-1
2-(4-chloro-2-methoxyphenyl)-4-methylthiazole-5-carboxylic acid

: 1354397-05-9
[2-(4-chloro-2-methoxyphenyl)-4-methylthiazol-5-yl]carbamic acid 1,2,3,4-tetrahydrobenzo[4,5]imidazo[1,2-a]pyridin-7-ylmethyl ester

Guidance literature:: With diphenyl phosphoryl azide; triethylamine; In toluene; for 2h; Reflux;

Reference yield:

: 27429-77-2
ethyl 1,2,3,4-tetrahydrobenzo[4,5]imidazo[1,2-a]pyridine-7-carboxylate

: 1354397-05-9
[2-(4-chloro-2-methoxyphenyl)-4-methylthiazol-5-yl]carbamic acid 1,2,3,4-tetrahydrobenzo[4,5]imidazo[1,2-a]pyridin-7-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / Cooling with ice

2: diphenyl phosphoryl azide; triethylamine / toluene / 2 h / Reflux

With lithium aluminium tetrahydride; diphenyl phosphoryl azide; triethylamine; In tetrahydrofuran; toluene;

Reference yield:

: 453-71-4
3-nitro-4-fluorobenzoic acid

: 1354397-05-9
[2-(4-chloro-2-methoxyphenyl)-4-methylthiazol-5-yl]carbamic acid 1,2,3,4-tetrahydrobenzo[4,5]imidazo[1,2-a]pyridin-7-ylmethyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: sulfuric acid / 8 h / Reflux

2: triethylamine / ethanol / 2 h / 20 °C / Cooling with ice

3: 5%-palladium/activated carbon; hydrogen / methanol / 20 °C

4: dihydrogen peroxide; formic acid / 0.67 h / Reflux

5: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / Cooling with ice

6: diphenyl phosphoryl azide; triethylamine / toluene / 2 h / Reflux

With lithium aluminium tetrahydride; formic acid; sulfuric acid; diphenyl phosphoryl azide; 5%-palladium/activated carbon; hydrogen; dihydrogen peroxide; triethylamine; In tetrahydrofuran; methanol; ethanol; toluene;