C₂₉H₃₄O₆S

Base Information

• Chemical Name: C₂₉H₃₄O₆S
• CAS No.: 1256640-02-4
• Molecular Formula: C₂₉H₃₄O₆S
• Molecular Weight: 510.651
• Mol file: 1256640-02-4.mol

Synonyms:C₂₉H₃₄O₆S

Chemical Property of C₂₉H₃₄O₆S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₉H₃₄O₆S

There total 9 articles about C₂₉H₃₄O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

C22H28O4 (1256640-01-3) + p-toluenesulfonyl chloride (98-59-9) → C29H34O6S (1256640-02-4)

Guidance literature:

With di(n-butyl)tin oxide; triethylamine; In dichloromethane; at 20 ℃; for 3h; regioselective reaction; Inert atmosphere;

DOI:10.1021/ol102390t

Reference yield:

C20H22O4 (1256639-98-1) → C29H34O6S (1256640-02-4)

Guidance literature:

Multi-step reaction with 4 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / -10 - 20 °C / Inert atmosphere

2: titanium(IV) isopropylate; tert.-butylhydroperoxide; N,N-Diisopropyltryptamine / decane; dichloromethane / -30 - -25 °C / Molecular sieve; Inert atmosphere

3: tetrahydrofuran / 1.83 h / -40 - 20 °C / Inert atmosphere

4: di(n-butyl)tin oxide; triethylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere

With titanium(IV) isopropylate; tert.-butylhydroperoxide; lithium aluminium tetrahydride; N,N-Diisopropyltryptamine; di(n-butyl)tin oxide; triethylamine; In tetrahydrofuran; decane; dichloromethane; 2: Sharpless epoxidation;

DOI:10.1021/ol102390t

Reference yield:

C19H22O3 (1256639-99-2) → C29H34O6S (1256640-02-4)

Guidance literature:

Multi-step reaction with 3 steps

1: titanium(IV) isopropylate; tert.-butylhydroperoxide; N,N-Diisopropyltryptamine / decane; dichloromethane / -30 - -25 °C / Molecular sieve; Inert atmosphere

2: tetrahydrofuran / 1.83 h / -40 - 20 °C / Inert atmosphere

3: di(n-butyl)tin oxide; triethylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere

With titanium(IV) isopropylate; tert.-butylhydroperoxide; N,N-Diisopropyltryptamine; di(n-butyl)tin oxide; triethylamine; In tetrahydrofuran; decane; dichloromethane; 1: Sharpless epoxidation;

DOI:10.1021/ol102390t

upstream raw materials:

C₁₉H₂₂O₄

C₂₂H₂₈O₄

p-toluenesulfonyl chloride

C₂₀H₂₂O₄

Downstream raw materials:

C₂₉H₃₆O₈S

C₂₈H₃₂O₇S

C₂₈H₃₀O₆S

C₂₁H₂₄O₆S