Benzoic acid (Z)-4-dimethylamino-2-oxo-3-phenylsulfanyl-but-3-enyl ester

Base Information

Chemical Name:Benzoic acid (Z)-4-dimethylamino-2-oxo-3-phenylsulfanyl-but-3-enyl ester
CAS No.:115412-95-8
Molecular Formula:C₁₉H₁₉NO₃S
Molecular Weight:341.431
Hs Code.:

Synonyms:Benzoic acid (Z)-4-dimethylamino-2-oxo-3-phenylsulfanyl-but-3-enyl ester

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Chemical Property of Benzoic acid (Z)-4-dimethylamino-2-oxo-3-phenylsulfanyl-but-3-enyl ester

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Technology Process of Benzoic acid (Z)-4-dimethylamino-2-oxo-3-phenylsulfanyl-but-3-enyl ester

There total 5 articles about Benzoic acid (Z)-4-dimethylamino-2-oxo-3-phenylsulfanyl-but-3-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 4637-24-5
N,N-dimethyl-formamide dimethyl acetal

: 115413-22-4
Benzoic acid 2-oxo-3-phenylsulfanyl-propyl ester

: 115412-95-8
Benzoic acid (Z)-4-dimethylamino-2-oxo-3-phenylsulfanyl-but-3-enyl ester

Guidance literature:: at 70 ℃; for 1.5h;
DOI:10.1055/s-1987-28113

Reference yield:

: 5296-21-9
2-(phenylsulfanylmethyl)oxirane

: 115412-95-8
Benzoic acid (Z)-4-dimethylamino-2-oxo-3-phenylsulfanyl-but-3-enyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 18 percent / Bu₄NCl / toluene / 6 h / Heating

2: 61 percent / DMSO, acetic anhydride / 24 h / Ambient temperature

3: 83 percent / 1.5 h / 70 °C

With acetic anhydride; dimethyl sulfoxide; tetrabutyl-ammonium chloride; In toluene;
DOI:10.1055/s-1987-28113

Reference yield:

: 3111-52-2
potassium thiophenolate

: 115412-95-8
Benzoic acid (Z)-4-dimethylamino-2-oxo-3-phenylsulfanyl-but-3-enyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 78 percent / aq. ethanol / 0.5 h

2: 18 percent / Bu₄NCl / toluene / 6 h / Heating

3: 61 percent / DMSO, acetic anhydride / 24 h / Ambient temperature

4: 83 percent / 1.5 h / 70 °C

With acetic anhydride; dimethyl sulfoxide; tetrabutyl-ammonium chloride; In ethanol; toluene;
DOI:10.1055/s-1987-28113