12-Benzyl-1,6,7,12b-tetrahydro-4-oxo-2-(1-pyrrolidinyl)-4H-indolo<2,3-a>quinolizine

Base Information

Chemical Name:12-Benzyl-1,6,7,12b-tetrahydro-4-oxo-2-(1-pyrrolidinyl)-4H-indolo<2,3-a>quinolizine
CAS No.:85222-93-1
Molecular Formula:C₂₆H₂₇N₃O
Molecular Weight:397.52
Hs Code.:

Synonyms:12-Benzyl-1,6,7,12b-tetrahydro-4-oxo-2-(1-pyrrolidinyl)-4H-indolo<2,3-a>quinolizine

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Chemical Property of 12-Benzyl-1,6,7,12b-tetrahydro-4-oxo-2-(1-pyrrolidinyl)-4H-indolo<2,3-a>quinolizine

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Technology Process of 12-Benzyl-1,6,7,12b-tetrahydro-4-oxo-2-(1-pyrrolidinyl)-4H-indolo<2,3-a>quinolizine

There total 2 articles about 12-Benzyl-1,6,7,12b-tetrahydro-4-oxo-2-(1-pyrrolidinyl)-4H-indolo<2,3-a>quinolizine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85222-84-0
(E)-4-(2,9-Dibenzyl-2,3,4,9-tetrahydro-1H-β-carbolin-1-yl)-3-methoxy-but-2-enoic acid methyl ester

: 85222-93-1
12-Benzyl-1,6,7,12b-tetrahydro-4-oxo-2-(1-pyrrolidinyl)-4H-indolo<2,3-a>quinolizine

Guidance literature:: Multi-step reaction with 3 steps

2: 100 percent / 2 N HCl / tetrahydrofuran / 2 h / Heating

3: benzene / 1 h / Heating

With hydrogenchloride; In tetrahydrofuran; benzene;
DOI:10.1021/jo00158a010

Reference yield:

: 85222-68-0
2,9-Dibenzyl-4,9-dihydro-3H-β-carbolin-2-ium; bromide

: 85222-93-1
12-Benzyl-1,6,7,12b-tetrahydro-4-oxo-2-(1-pyrrolidinyl)-4H-indolo<2,3-a>quinolizine

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / zinc powder / acetonitrile / 1) cooling with an ice-salt bath -> room temperature, 5 h, 2) room temp., 2 days

3: 100 percent / 2 N HCl / tetrahydrofuran / 2 h / Heating

4: benzene / 1 h / Heating

With hydrogenchloride; zinc; In tetrahydrofuran; acetonitrile; benzene;
DOI:10.1021/jo00158a010