6-(4-Methoxyphenyl)-4-tert-butyl-2-methyl-4-(1-propinyl)-4H-1,4-oxaphosphorin-4-ium-bromid

Base Information

Chemical Name:6-(4-Methoxyphenyl)-4-tert-butyl-2-methyl-4-(1-propinyl)-4H-1,4-oxaphosphorin-4-ium-bromid
CAS No.:85472-46-4
Molecular Formula:Br*C₁₉H₂₄O₂P
Molecular Weight:395.276
Hs Code.:

Synonyms:6-(4-Methoxyphenyl)-4-tert-butyl-2-methyl-4-(1-propinyl)-4H-1,4-oxaphosphorin-4-ium-bromid

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Chemical Property of 6-(4-Methoxyphenyl)-4-tert-butyl-2-methyl-4-(1-propinyl)-4H-1,4-oxaphosphorin-4-ium-bromid

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Technology Process of 6-(4-Methoxyphenyl)-4-tert-butyl-2-methyl-4-(1-propinyl)-4H-1,4-oxaphosphorin-4-ium-bromid

There total 1 articles about 6-(4-Methoxyphenyl)-4-tert-butyl-2-methyl-4-(1-propinyl)-4H-1,4-oxaphosphorin-4-ium-bromid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 55523-26-7
tert-Butyldi(1-propynyl)phosphane

: 2632-13-5
2-Bromo-4'-methoxyacetophenone

: 85472-46-4
6-(4-Methoxyphenyl)-4-tert-butyl-2-methyl-4-(1-propinyl)-4H-1,4-oxaphosphorin-4-ium-bromid

Guidance literature:: In chloroform; for 24h;

Reference yield: 75.0%

: 85472-46-4
6-(4-Methoxyphenyl)-4-tert-butyl-2-methyl-4-(1-propinyl)-4H-1,4-oxaphosphorin-4-ium-bromid

: 85472-48-6
6-(4-Methoxypheny)-4-tert-butyl-2-methyl-4H-1,4-oxaphosphorin-4-oxid

Guidance literature:: With sodium hydroxide; In ethanol; for 12h; Heating;

Reference yield:

: 85472-46-4
6-(4-Methoxyphenyl)-4-tert-butyl-2-methyl-4-(1-propinyl)-4H-1,4-oxaphosphorin-4-ium-bromid

: 85472-50-0
1-tert-Butyl-1,6-dihydro-5-(4-methoxyphenyl)-3(2H)-phosphorinon-1-oxid

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / 20percent NaOH / ethanol / 12 h / Heating

2: 83 percent / conc. HCl / 24 h / Heating

With hydrogenchloride; sodium hydroxide; In ethanol;