Technology Process of (2-benzoyl-5-methoxyphenyl)(p-tolyl)methanone
There total 3 articles about (2-benzoyl-5-methoxyphenyl)(p-tolyl)methanone which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C22H21NO;
With
oxygen; copper diacetate;
In
diethyl ether; N,N-dimethyl-formamide;
at 80 ℃;
With
hydrogenchloride;
In
diethyl ether; water; N,N-dimethyl-formamide;
at 80 ℃;
DOI:10.1021/ol200425c
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: diethyl ether / 2 h / 60 °C / Cooling; Sealed tube
2.1: oxygen; copper diacetate / diethyl ether; N,N-dimethyl-formamide / 80 °C
2.2: 80 °C
With
oxygen; copper diacetate;
In
diethyl ether; N,N-dimethyl-formamide;
DOI:10.1021/ol200425c
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 100 °C
2.1: potassium phosphate; palladium diacetate; triphenylphosphine / toluene / 80 °C / Inert atmosphere
3.1: diethyl ether / 2 h / 60 °C / Cooling; Sealed tube
4.1: oxygen; copper diacetate / diethyl ether; N,N-dimethyl-formamide / 80 °C
4.2: 80 °C
With
potassium phosphate; N-Bromosuccinimide; oxygen; copper diacetate; palladium diacetate; triphenylphosphine; dibenzoyl peroxide;
In
tetrachloromethane; diethyl ether; N,N-dimethyl-formamide; toluene;
2.1: Suzuki coupling;
DOI:10.1021/ol200425c
