(R)-benzyl 1-hydroxy-3-(trifluoromethylsulfonamido)propan-2-ylcarbamate

Base Information

• Chemical Name: (R)-benzyl 1-hydroxy-3-(trifluoromethylsulfonamido)propan-2-ylcarbamate
• CAS No.: 1224962-36-0
• Molecular Formula: C₁₂H₁₅F₃N₂O₅S
• Molecular Weight: 356.323

Synonyms:(R)-benzyl 1-hydroxy-3-(trifluoromethylsulfonamido)propan-2-ylcarbamate

Chemical Property of (R)-benzyl 1-hydroxy-3-(trifluoromethylsulfonamido)propan-2-ylcarbamate

Chemical Property:

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Technology Process of (R)-benzyl 1-hydroxy-3-(trifluoromethylsulfonamido)propan-2-ylcarbamate

There total 1 articles about (R)-benzyl 1-hydroxy-3-(trifluoromethylsulfonamido)propan-2-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl (R)-1-(tetrahydro-2H-pyran-2-yloxy)-3-(trifluoromethylsulfonamido)propan-2-ylcarbamate (1224962-35-9) → (R)-benzyl 1-hydroxy-3-(trifluoromethylsulfonamido)propan-2-ylcarbamate (1224962-36-0)

Guidance literature:

With toluene-4-sulfonic acid; In methanol; at 20 ℃; for 4h;

DOI:10.1039/b919549a

Reference yield: 90.0%

triisopropylsilyl chloride (13154-24-0) + (R)-benzyl 1-hydroxy-3-(trifluoromethylsulfonamido)propan-2-ylcarbamate (1224962-36-0) → (R)-benzyl 3-(trifluoromethylsulfonamido)-1-(triisopropylsilyloxy)propan-2-ylcarbamate (1224962-38-2)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; for 5h;

DOI:10.1039/b919549a

Reference yield: 86.0%

(R)-benzyl 1-hydroxy-3-(trifluoromethylsulfonamido)propan-2-ylcarbamate (1224962-36-0) + tert-butylchlorodiphenylsilane (58479-61-1) → (R)-benzy l1-(tert-butyldiphenylsilyloxy)-3-(trifluoromethylsulfonamido)propan-2-ylcarbamate (1224962-39-3)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; for 5h;

DOI:10.1039/b919549a

upstream raw materials:

benzyl (R)-1-(tetrahydro-2H-pyran-2-yloxy)-3-(trifluoromethylsulfonamido)propan-2-ylcarbamate

Downstream raw materials:

(R)-benzyl 3-(trifluoromethylsulfonamido)-1-(triisopropylsilyloxy)propan-2-ylcarbamate

(R)-benzyl 1-(tert-butyldimethylsilyloxy)-3-(trifluoromethylsulfonamido)propan-2-ylcarbamate

(R)-benzy l1-(tert-butyldiphenylsilyloxy)-3-(trifluoromethylsulfonamido)propan-2-ylcarbamate

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