28-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate 3-O-2,3,4,6-tetra-O-benzoyl-β-D-galactopyranoside

Base Information

• Chemical Name: 28-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate 3-O-2,3,4,6-tetra-O-benzoyl-β-D-galactopyranoside
• CAS No.: 1609983-92-7
• Molecular Formula: C₁₀₆H₁₀₇NO₂₂
• Molecular Weight: 1747.01
• Mol file: 1609983-92-7.mol

Synonyms:28-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate 3-O-2,3,4,6-tetra-O-benzoyl-β-D-galactopyranoside

Chemical Property of 28-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate 3-O-2,3,4,6-tetra-O-benzoyl-β-D-galactopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 28-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate 3-O-2,3,4,6-tetra-O-benzoyl-β-D-galactopyranoside

There total 1 articles about 28-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate 3-O-2,3,4,6-tetra-O-benzoyl-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate (1609983-87-0) + C36H28Cl3NO9 → 28-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate 3-O-2,3,4,6-tetra-O-benzoyl-β-D-galactopyranoside (1609983-92-7)

Guidance literature:

6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate; C₃₆H₂₈Cl₃NO₉; In dichloromethane; at 20 ℃; for 0.5h; Molecular sieve;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -30 - 20 ℃; for 1.5h; Molecular sieve;

DOI:10.1016/j.ejmech.2014.03.080

Reference yield:

28-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate 3-O-2,3,4,6-tetra-O-benzoyl-β-D-galactopyranoside (1609983-92-7) → C99H101NO22

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In methanol; dichloromethane; for 5h; under 760.051 Torr;

DOI:10.1016/j.ejmech.2014.03.080

upstream raw materials:

6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate