(S)-2-{(R)-2-benzyloxycarbonylamino-3-[(R)-2-benzyloxycarbonylamino-2-((S)-1-carboxyethylcarbamoyl)ethyldisulfanyl]propionylamino}propionic acid

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Chemical Name:(S)-2-{(R)-2-benzyloxycarbonylamino-3-[(R)-2-benzyloxycarbonylamino-2-((S)-1-carboxyethylcarbamoyl)ethyldisulfanyl]propionylamino}propionic acid
CAS No.:16217-52-0
Molecular Formula:C₂₈H₃₄N₄O₁₀S₂
Molecular Weight:650.731
Hs Code.:

(S)-2-{(R)-2-benzyloxycarbonylamino-3-[(R)-2-benzyloxycarbonylamino-2-((S)-1-carboxyethylcarbamoyl)ethyldisulfanyl]propionylamino}propionic acid

Synonyms:(S)-2-{(R)-2-benzyloxycarbonylamino-3-[(R)-2-benzyloxycarbonylamino-2-((S)-1-carboxyethylcarbamoyl)ethyldisulfanyl]propionylamino}propionic acid

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Chemical Property of (S)-2-{(R)-2-benzyloxycarbonylamino-3-[(R)-2-benzyloxycarbonylamino-2-((S)-1-carboxyethylcarbamoyl)ethyldisulfanyl]propionylamino}propionic acid

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Technology Process of (S)-2-{(R)-2-benzyloxycarbonylamino-3-[(R)-2-benzyloxycarbonylamino-2-((S)-1-carboxyethylcarbamoyl)ethyldisulfanyl]propionylamino}propionic acid

There total 3 articles about (S)-2-{(R)-2-benzyloxycarbonylamino-3-[(R)-2-benzyloxycarbonylamino-2-((S)-1-carboxyethylcarbamoyl)ethyldisulfanyl]propionylamino}propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 886981-18-6
benzyl N-[(1R)-1-({[(2R)-2-(benzylcarbonyl)amino-3-(1H-1,2,3-benzotriazol-1-yl)-3-oxopropyl]disulfanyl}methyl)-2-(1H-1,2,3-benzotriazol-1-yl)-2-oxoethyl]carbamate

: 56-41-7,25191-17-7,18875-37-1
L-alanin

: 16217-52-0
(S)-2-{(R)-2-benzyloxycarbonylamino-3-[(R)-2-benzyloxycarbonylamino-2-((S)-1-carboxyethylcarbamoyl)ethyldisulfanyl]propionylamino}propionic acid

Guidance literature:: With triethylamine; In water; acetonitrile; at 20 ℃; for 1h;
DOI:10.1055/s-2006-926287

Reference yield:

: N,N'-(N,N'-bis-benzyloxycarbonyl-L-cystyl)-bis-L-alanine diethyl ester

: 16217-52-0
(S)-2-{(R)-2-benzyloxycarbonylamino-3-[(R)-2-benzyloxycarbonylamino-2-((S)-1-carboxyethylcarbamoyl)ethyldisulfanyl]propionylamino}propionic acid

Guidance literature:: With 1,4-dioxane; sodium hydroxide;
DOI:10.1007/BF00898707

Reference yield:

: 6968-11-2
N,N'-bis(benzyloxycarbonyl)-L-cystine

: 16217-52-0
(S)-2-{(R)-2-benzyloxycarbonylamino-3-[(R)-2-benzyloxycarbonylamino-2-((S)-1-carboxyethylcarbamoyl)ethyldisulfanyl]propionylamino}propionic acid

Guidance literature:: Multi-step reaction with 2 steps

1: tripropylamine; chlorocarbonic acid ethyl ester; THF / anschliessend Behandeln mit L-Alanin-aethylester

2: dioxane; aqueous NaOH

With tetrahydrofuran; 1,4-dioxane; tri-n-propylamine; sodium hydroxide; chloroformic acid ethyl ester;
DOI:10.1007/BF00898707