(5R,10R)-(-)-3-methyl-3-<1-acetyl-3-(1-methylethylidene)cyclopentyl>propyl mesitoate

Base Information

Chemical Name:(5R,10R)-(-)-3-methyl-3-<1-acetyl-3-(1-methylethylidene)cyclopentyl>propyl mesitoate
CAS No.:117711-45-2
Molecular Formula:C₂₄H₃₄O₃
Molecular Weight:370.532
Hs Code.:

Synonyms:(5R,10R)-(-)-3-methyl-3-<1-acetyl-3-(1-methylethylidene)cyclopentyl>propyl mesitoate

Suppliers and Price of (5R,10R)-(-)-3-methyl-3-<1-acetyl-3-(1-methylethylidene)cyclopentyl>propyl mesitoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (5R,10R)-(-)-3-methyl-3-<1-acetyl-3-(1-methylethylidene)cyclopentyl>propyl mesitoate

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Technology Process of (5R,10R)-(-)-3-methyl-3-<1-acetyl-3-(1-methylethylidene)cyclopentyl>propyl mesitoate

There total 4 articles about (5R,10R)-(-)-3-methyl-3-<1-acetyl-3-(1-methylethylidene)cyclopentyl>propyl mesitoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 42091-47-4
2-Isopropylidenebutane-1,4-diol

: 117711-45-2
(5R,10R)-(-)-3-methyl-3-<1-acetyl-3-(1-methylethylidene)cyclopentyl>propyl mesitoate

Guidance literature:: Multi-step reaction with 3 steps

1: PBr₃ / diethyl ether / 0 - 20 °C

3: 2.) 4-(N,N-dimethylamino)pyridine / 1.) THF, Et₂O, RT, 1.5 h, 2.) RT, overnight

With dmap; phosphorus tribromide; In diethyl ether;
DOI:10.1021/jo00261a008

Reference yield:

: 85221-99-4
2-methyl-3-(bromomethyl)-5-bromo-2-pentene

: 117711-45-2
(5R,10R)-(-)-3-methyl-3-<1-acetyl-3-(1-methylethylidene)cyclopentyl>propyl mesitoate

Guidance literature:: Multi-step reaction with 2 steps

2: 2.) 4-(N,N-dimethylamino)pyridine / 1.) THF, Et₂O, RT, 1.5 h, 2.) RT, overnight

With dmap;
DOI:10.1021/jo00261a008

Reference yield:

: 117711-44-1
(S)-(+)-p-anisylpentenolide sulfoxide

: 117711-45-2
(5R,10R)-(-)-3-methyl-3-<1-acetyl-3-(1-methylethylidene)cyclopentyl>propyl mesitoate

Guidance literature:: Multi-step reaction with 3 steps

3: 2.) 4-(N,N-dimethylamino)pyridine / 1.) THF, Et₂O, RT, 1.5 h, 2.) RT, overnight

With dmap;
DOI:10.1021/jo00261a008