C₃₁H₃₃N₃O₈

Base Information

Chemical Name:C₃₁H₃₃N₃O₈
CAS No.:194042-14-3
Molecular Formula:C₃₁H₃₃N₃O₈
Molecular Weight:575.618
Hs Code.:

C<sub>31</sub>H<sub>33</sub>N<sub>3</sub>O<sub>8</sub>

Synonyms:C₃₁H₃₃N₃O₈

Suppliers and Price of C₃₁H₃₃N₃O₈

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₁H₃₃N₃O₈

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₁H₃₃N₃O₈

There total 24 articles about C₃₁H₃₃N₃O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 194042-13-2
C₃₈H₃₉N₃O₁₀S

: 194042-14-3
C₃₁H₃₃N₃O₈

Guidance literature:: With sodium naphthalenide; In 1,2-dimethoxyethane; at -70 ℃;
DOI:10.1016/S0040-4020(97)00652-2

Reference yield:

: 177957-70-9
{3-Benzyloxy-5-benzyloxymethoxymethyl-2-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-phenyl}-carbamic acid allyl ester

: 194042-14-3
C₃₁H₃₃N₃O₈

Guidance literature:: Multi-step reaction with 24 steps

1: 99 percent / NaH / paraffin; tetrahydrofuran / 1.) -78 deg C -> room temperature, 4 h, 2.) room temperature, 2 h

2: 21.2 g / Zn, AcOH / tetrahydrofuran; H₂O / 1 h / Ambient temperature

3: Et₃N / dimethylformamide / 4 h / Ambient temperature

4: 92 percent / Et₃N / CH₂Cl₂ / 3 h / Ambient temperature

5: 94 percent / NaH, imidazole / paraffin; tetrahydrofuran / Heating

6: 98 percent / (HF)n*Py / 0.67 h / -10 °C

7: 95 percent / Dess-Martin periodinane / CH₂Cl₂ / 1 h / Ambient temperature

8: 1.) LiN(TMS)2, 2.) NaBH₄ / 1.) THF, -78 deg C -> -5 deg C, 3 h, 2.) H₂O, 0 deg C, 20 min

9: 80 percent / Et₃N, DMAP / CH₂Cl₂ / Ambient temperature

10: 95 percent / Dess-Martin periodinane / CH₂Cl₂ / 1 h / Ambient temperature

11: 94 percent / (HF)n*Py / Ambient temperature

12: 63 percent / DBU / tetrahydrofuran / Ambient temperature

13: 88 percent / NaBH₄ / tetrahydrofuran; H₂O / 1 h / Ambient temperature

14: 75 percent / Et₃N, DMAP / CH₂Cl₂ / 7 h / Ambient temperature

15: 85 percent / Ph₃P, Pd(PPh₃, octanoic acid / tetrahydrofuran / Ambient temperature

16: 66 percent / MCPBA / CH₂Cl₂ / 0 °C

17: 66 percent / NaHCO₃ / 5 h / -5 - 10 °C

18: 90 percent / Dess-Martin periodinane / CH₂Cl₂ / 0.33 h / Ambient temperature

19: 85 percent / (HF)n*Py / 1.) -10 deg C -> room temperature, 2.) room temperature, 2 h

20: 88 percent / K₂CO₃ / methanol / 0 - 20 °C

21: 88 percent / pyridine / 0 - 20 °C

22: 93 percent / NH₃ / tetrahydrofuran / 8 h / Ambient temperature

23: 85 percent / DMAP / pyridine / 15 h / Ambient temperature

24: 61 percent / sodium naphthalenide / 1,2-dimethoxy-ethane / -70 °C

With 1H-imidazole; dmap; sodium tetrahydroborate; Octanoic acid; (HF)n*Py; Pd(PPh₃; ammonia; sodium naphthalenide; sodium hydride; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; lithium hexamethyldisilazane; zinc; In tetrahydrofuran; pyridine; methanol; 1,2-dimethoxyethane; dichloromethane; water; N,N-dimethyl-formamide; paraffin;
DOI:10.1016/S0040-4020(97)00652-2

Reference yield:

: 194042-12-1
C₃₆H₃₇N₃O₉S

: 194042-14-3
C₃₁H₃₃N₃O₈

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / DMAP / pyridine / 15 h / Ambient temperature

2: 61 percent / sodium naphthalenide / 1,2-dimethoxy-ethane / -70 °C

With dmap; sodium naphthalenide; In pyridine; 1,2-dimethoxyethane;
DOI:10.1016/S0040-4020(97)00652-2