5,7-bis(benzyloxy)-2-(4-benzyloxyphenyl)-3-((1R,5R)-5-methyl-4-oxocyclohex-2-enyloxy)4H-chromen-4-one

Base Information

Chemical Name:5,7-bis(benzyloxy)-2-(4-benzyloxyphenyl)-3-((1R,5R)-5-methyl-4-oxocyclohex-2-enyloxy)4H-chromen-4-one
CAS No.:1232680-31-7
Molecular Formula:C₄₃H₃₆O₇
Molecular Weight:664.755
Hs Code.:

Synonyms:5,7-bis(benzyloxy)-2-(4-benzyloxyphenyl)-3-((1R,5R)-5-methyl-4-oxocyclohex-2-enyloxy)4H-chromen-4-one

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Chemical Property of 5,7-bis(benzyloxy)-2-(4-benzyloxyphenyl)-3-((1R,5R)-5-methyl-4-oxocyclohex-2-enyloxy)4H-chromen-4-one

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Technology Process of 5,7-bis(benzyloxy)-2-(4-benzyloxyphenyl)-3-((1R,5R)-5-methyl-4-oxocyclohex-2-enyloxy)4H-chromen-4-one

There total 1 articles about 5,7-bis(benzyloxy)-2-(4-benzyloxyphenyl)-3-((1R,5R)-5-methyl-4-oxocyclohex-2-enyloxy)4H-chromen-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 23405-70-1
5,7-bis(benzyloxy)-2-(4-(benzyloxy)phenyl)-3-hydroxy-4H-chromen-4-one

: 1092513-38-6
tert-butyl (1R,5R)-5-methyl-4-oxocyclohex-2-enyl carbonate

: 1232680-31-7
5,7-bis(benzyloxy)-2-(4-benzyloxyphenyl)-3-((1R,5R)-5-methyl-4-oxocyclohex-2-enyloxy)4H-chromen-4-one

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; triphenylphosphine; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ol101009q

Reference yield:

: 1232680-31-7
5,7-bis(benzyloxy)-2-(4-benzyloxyphenyl)-3-((1R,5R)-5-methyl-4-oxocyclohex-2-enyloxy)4H-chromen-4-one

: 1232680-32-8
5,7-bis(benzyloxy)-2-(4-benzyloxyphenyl)-3-((1R,4S,5R)-4-hydroxy-5-methylcyclohex-2-enyloxy)-4H-chromen-4-one

: C₄₃H₃₈O₇

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at -78 ℃; for 1h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ol101009q