methyl 2-O-acetyl-4-O-(2,3,4-tri-O-acetyl-β-D-xylopyranosyl)-3-O-(2,3,5-tri-O-benzoyl-α-L-arabinofuranosyl)-β-D-xylopyranoside

Base Information

Chemical Name:methyl 2-O-acetyl-4-O-(2,3,4-tri-O-acetyl-β-D-xylopyranosyl)-3-O-(2,3,5-tri-O-benzoyl-α-L-arabinofuranosyl)-β-D-xylopyranoside
CAS No.:93396-82-8
Molecular Formula:C₄₅H₄₈O₂₀
Molecular Weight:908.864
Hs Code.:

Synonyms:methyl 2-O-acetyl-4-O-(2,3,4-tri-O-acetyl-β-D-xylopyranosyl)-3-O-(2,3,5-tri-O-benzoyl-α-L-arabinofuranosyl)-β-D-xylopyranoside

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Chemical Property of methyl 2-O-acetyl-4-O-(2,3,4-tri-O-acetyl-β-D-xylopyranosyl)-3-O-(2,3,5-tri-O-benzoyl-α-L-arabinofuranosyl)-β-D-xylopyranoside

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Technology Process of methyl 2-O-acetyl-4-O-(2,3,4-tri-O-acetyl-β-D-xylopyranosyl)-3-O-(2,3,5-tri-O-benzoyl-α-L-arabinofuranosyl)-β-D-xylopyranoside

There total 4 articles about methyl 2-O-acetyl-4-O-(2,3,4-tri-O-acetyl-β-D-xylopyranosyl)-3-O-(2,3,5-tri-O-benzoyl-α-L-arabinofuranosyl)-β-D-xylopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.1%

: 42868-96-2
2,3,5-tri-O-benzoyl-α-L-arabinofuranosyl bromide

: 93396-81-7
methyl 2-O-acetyl-4-O-(2,3,4-tri-O-acetyl-β-D-xylopyranosyl)-β-D-xylopyranoside

: 93396-82-8
methyl 2-O-acetyl-4-O-(2,3,4-tri-O-acetyl-β-D-xylopyranosyl)-3-O-(2,3,5-tri-O-benzoyl-α-L-arabinofuranosyl)-β-D-xylopyranoside

Guidance literature:: With mercury(II) cyanide; In benzene; for 3h;
DOI:10.1016/0008-6215(84)85243-X

Reference yield:

: 63911-03-5
methyl 2,3-anhydro-4-O-β-D-xylopyranosyl-β-D-ribopyranoside

: 93396-82-8
methyl 2-O-acetyl-4-O-(2,3,4-tri-O-acetyl-β-D-xylopyranosyl)-3-O-(2,3,5-tri-O-benzoyl-α-L-arabinofuranosyl)-β-D-xylopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / sodium hydride / 1.5 h / 100 °C

2: 89.7 percent / pyridine / 6 h / Ambient temperature

3: 92.4 percent / H₂ / 5 percent Pd/C / acetone; methanol / 5 h / Ambient temperature

4: 96.1 percent / mercuric cyanide / benzene / 3 h

With pyridine; hydrogen; mercury(II) cyanide; sodium hydride; palladium on activated charcoal; In methanol; acetone; benzene;
DOI:10.1016/0008-6215(84)85243-X

Reference yield:

: 93396-79-3
methyl 3-O-benzyl-4-O-β-D-xylopyranosyl-β-D-xylopyranoside

: 93396-82-8
methyl 2-O-acetyl-4-O-(2,3,4-tri-O-acetyl-β-D-xylopyranosyl)-3-O-(2,3,5-tri-O-benzoyl-α-L-arabinofuranosyl)-β-D-xylopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 89.7 percent / pyridine / 6 h / Ambient temperature

2: 92.4 percent / H₂ / 5 percent Pd/C / acetone; methanol / 5 h / Ambient temperature

3: 96.1 percent / mercuric cyanide / benzene / 3 h

With pyridine; hydrogen; mercury(II) cyanide; palladium on activated charcoal; In methanol; acetone; benzene;
DOI:10.1016/0008-6215(84)85243-X