N-methyl-α-phenylmalonamic acid

Base Information

Chemical Name:N-methyl-α-phenylmalonamic acid
CAS No.:7713-73-7
Molecular Formula:C₁₀H₁₁NO₃
Molecular Weight:193.202
Hs Code.:

Synonyms:N-methyl-α-phenylmalonamic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-methyl-α-phenylmalonamic acid

Chemical Property:

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Technology Process of N-methyl-α-phenylmalonamic acid

There total 6 articles about N-methyl-α-phenylmalonamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 103-82-2
phenylacetic acid

: 624-83-9
methyl isocyanate

: 7713-73-7
N-methyl-α-phenylmalonamic acid

Guidance literature:: With isopropylmagnesium chloride;
DOI:10.1021/ja01623a049

Reference yield:

: 7713-74-8
ethyl 3-(methylamino)-3-oxo-2-phenylpropanoate

: 7713-73-7
N-methyl-α-phenylmalonamic acid

Guidance literature:: With sodium hydroxide; In ethanol; Ambient temperature;

Reference yield:

: 17097-90-4
2-phenylmalonic acid monoethyl ester

: 7713-73-7
N-methyl-α-phenylmalonamic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 18.6 g / thionyl chloride / CH₂Cl₂ / 20 h / Ambient temperature

2: pyridine / CH₂Cl₂ / 0 °C

3: sodium hydroxide / aq. ethanol / Ambient temperature

With pyridine; sodium hydroxide; thionyl chloride; In ethanol; dichloromethane;