2-(4-(difluoromethoxy)-3-methylphenyl)-1-(3-methylphenyl)-2-hydroxyethanone

Base Information

Chemical Name:2-(4-(difluoromethoxy)-3-methylphenyl)-1-(3-methylphenyl)-2-hydroxyethanone
CAS No.:1622220-02-3
Molecular Formula:C₁₇H₁₆F₂O₃
Molecular Weight:306.309
Hs Code.:

Synonyms:2-(4-(difluoromethoxy)-3-methylphenyl)-1-(3-methylphenyl)-2-hydroxyethanone

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Chemical Property of 2-(4-(difluoromethoxy)-3-methylphenyl)-1-(3-methylphenyl)-2-hydroxyethanone

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Technology Process of 2-(4-(difluoromethoxy)-3-methylphenyl)-1-(3-methylphenyl)-2-hydroxyethanone

There total 5 articles about 2-(4-(difluoromethoxy)-3-methylphenyl)-1-(3-methylphenyl)-2-hydroxyethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15174-69-3
4-hydroxy-3-methyl-benzaldehyde

: 1622220-02-3
2-(4-(difluoromethoxy)-3-methylphenyl)-1-(3-methylphenyl)-2-hydroxyethanone

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 3.25 h / 95 °C

2.1: n-butyllithium / tetrahydrofuran / 0.5 h / -29 - -10 °C / Inert atmosphere

2.2: 1.25 h / -29 - 20 °C

3.1: bis-[(trifluoroacetoxy)iodo]benzene / acetonitrile; water

With n-butyllithium; potassium carbonate; bis-[(trifluoroacetoxy)iodo]benzene; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 4-(difluoromethoxy)-3-methylbenzaldehyde

: 1622220-02-3
2-(4-(difluoromethoxy)-3-methylphenyl)-1-(3-methylphenyl)-2-hydroxyethanone

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran / 0.5 h / -29 - -10 °C / Inert atmosphere

1.2: 1.25 h / -29 - 20 °C

2.1: bis-[(trifluoroacetoxy)iodo]benzene / acetonitrile; water

With n-butyllithium; bis-[(trifluoroacetoxy)iodo]benzene; In tetrahydrofuran; water; acetonitrile;