Technology Process of C14H22N2O2*ClH
There total 3 articles about C14H22N2O2*ClH which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C14H20N2O4;
With
thiophene; hydrogen;
platinum on activated charcoal; vanadia;
In
di-isopropyl ether; ethyl acetate;
at 20 ℃;
for 20h;
With
hydrogenchloride;
In
di-isopropyl ether; isopropyl alcohol;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium carbonate / N,N-dimethyl acetamide / 16 h / 70 °C
2: thiophene; hydrogen / platinum on activated charcoal; vanadia / di-isopropyl ether; ethyl acetate / 20 h / 20 °C
With
thiophene; hydrogen; sodium carbonate;
platinum on activated charcoal; vanadia;
In
di-isopropyl ether; N,N-dimethyl acetamide; ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium carbonate / N,N-dimethyl acetamide / 16 h / 70 °C
2: thiophene; hydrogen / platinum on activated charcoal; vanadia / di-isopropyl ether; ethyl acetate / 20 h / 20 °C
With
thiophene; hydrogen; sodium carbonate;
platinum on activated charcoal; vanadia;
In
di-isopropyl ether; N,N-dimethyl acetamide; ethyl acetate;