Technology Process of C19H12Cl2FN7
There total 4 articles about C19H12Cl2FN7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine;
In
isopropyl alcohol;
at 90 ℃;
for 0.5h;
Microwave irradiation;
Sealed tube;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: copper diacetate; triethylamine / dichloromethane / 48 h / 20 °C / Molecular sieve
2: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 0.5 h / 90 °C / Microwave irradiation; Sealed tube
With
copper diacetate; triethylamine; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; isopropyl alcohol;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 4-Chloro-1,2-phenylenediamine / dichloromethane / 0.17 h / 20 °C
1.2: 20 °C
1.3: 2 h / 70 °C
2.1: hydrogenchloride / water; 1,4-dioxane / 20 °C
3.1: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 0.5 h / 90 °C / Microwave irradiation; Sealed tube
With
hydrogenchloride; 4-Chloro-1,2-phenylenediamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
1,4-dioxane; dichloromethane; water; isopropyl alcohol;