C₁₄H₂₃NO₆

Base Information

• Chemical Name: C₁₄H₂₃NO₆
• CAS No.: 1233402-45-3
• Molecular Formula: C₁₄H₂₃NO₆
• Molecular Weight: 301.34
• Mol file: 1233402-45-3.mol

Synonyms:C₁₄H₂₃NO₆

Chemical Property of C₁₄H₂₃NO₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₄H₂₃NO₆

There total 19 articles about C₁₄H₂₃NO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

C14H23NO6 → C14H23NO6 (1233402-45-3)

Guidance literature:

With sodium hydrogencarbonate; In tetrahydrofuran; water; at 0 - 20 ℃; for 4.16h;

Reference yield:

C15H26O5 (1257984-89-6) → C14H23NO6 (1233402-45-3)

Guidance literature:

Multi-step reaction with 8 steps

1.1: 1,4-diaza-bicyclo[2.2.2]octane / 72 h / 30 °C

1.2: 0.5 h / 20 °C

2.1: potassium hydroxide / ethanol / 4.5 h / 20 °C

3.1: ethanol; camphor-10-sulfonic acid / 24 h / 20 °C

4.1: periodic acid dihydrate / tetrahydrofuran / 0.5 h / 20 °C

5.1: sodium tetrahydroborate / tetrahydrofuran / 1 h / 20 °C

6.1: borane-dimethyl sulfide complex / dichloromethane / 1 h / 0 - 20 °C

6.2: 1 h / 0 - 20 °C

7.1: periodic acid dihydrate / tetrahydrofuran / 1 h / 0 °C

8.1: sodium hydrogencarbonate / water; tetrahydrofuran / 4.16 h / 0 - 20 °C

With 1,4-diaza-bicyclo[2.2.2]octane; sodium tetrahydroborate; periodic acid dihydrate; borane-dimethyl sulfide complex; ethanol; camphor-10-sulfonic acid; sodium hydrogencarbonate; potassium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; water;

Reference yield:

C22H36O8 (1257984-90-9) → C14H23NO6 (1233402-45-3)

Guidance literature:

Multi-step reaction with 7 steps

1.1: potassium hydroxide / ethanol / 4.5 h / 20 °C

2.1: ethanol; camphor-10-sulfonic acid / 24 h / 20 °C

3.1: periodic acid dihydrate / tetrahydrofuran / 0.5 h / 20 °C

4.1: sodium tetrahydroborate / tetrahydrofuran / 1 h / 20 °C

5.1: borane-dimethyl sulfide complex / dichloromethane / 1 h / 0 - 20 °C

5.2: 1 h / 0 - 20 °C

6.1: periodic acid dihydrate / tetrahydrofuran / 1 h / 0 °C

7.1: sodium hydrogencarbonate / water; tetrahydrofuran / 4.16 h / 0 - 20 °C

With sodium tetrahydroborate; periodic acid dihydrate; borane-dimethyl sulfide complex; ethanol; camphor-10-sulfonic acid; sodium hydrogencarbonate; potassium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; water;

upstream raw materials:

3,3-dimethoxypentane

C₁₅H₂₆O₅

C₂₂H₃₆O₈

C₁₀H₁₆O₆

Downstream raw materials:

ethyl (3R,4S,5R)-5-amino-3-(1-ethylpropoxy)-4-hydroxy-1-cyclohexene-1-carboxylate

Refernces