(S)-4-Methyl-2-[3-(1-methyl-cyclohexyl)-ureido]-pentanoic acid benzyl ester

Base Information

Chemical Name:(S)-4-Methyl-2-[3-(1-methyl-cyclohexyl)-ureido]-pentanoic acid benzyl ester
CAS No.:1027586-10-2
Molecular Formula:C₂₁H₃₂N₂O₃
Molecular Weight:360.497
Hs Code.:

Synonyms:(S)-4-Methyl-2-[3-(1-methyl-cyclohexyl)-ureido]-pentanoic acid benzyl ester

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Chemical Property of (S)-4-Methyl-2-[3-(1-methyl-cyclohexyl)-ureido]-pentanoic acid benzyl ester

Chemical Property:

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Technology Process of (S)-4-Methyl-2-[3-(1-methyl-cyclohexyl)-ureido]-pentanoic acid benzyl ester

There total 1 articles about (S)-4-Methyl-2-[3-(1-methyl-cyclohexyl)-ureido]-pentanoic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1123-25-7
1-methyl-1-cyclohexanecarboxylic acid

: 1738-77-8
L-leucine benzyl ester p-toluenesulfonate

: 1027586-10-2
(S)-4-Methyl-2-[3-(1-methyl-cyclohexyl)-ureido]-pentanoic acid benzyl ester

Guidance literature:: With 4-methyl-morpholine; diphenyl phosphoryl azide; Multistep reaction; 1.) toluene, 70 deg C, 2 h, 2.) toluene, RT, overnight;
DOI:10.1021/jm950592+

Reference yield:

: 1027586-10-2
(S)-4-Methyl-2-[3-(1-methyl-cyclohexyl)-ureido]-pentanoic acid benzyl ester

: 168471-10-1
N-(((1-methylcyclohexyl)amino)carbonyl)leucine

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 4h; Ambient temperature;
DOI:10.1021/jm950592+

Reference yield:

: 1027586-10-2
(S)-4-Methyl-2-[3-(1-methyl-cyclohexyl)-ureido]-pentanoic acid benzyl ester

: 5-Methyl-2-((R)-2-(1-methyl-1H-indol-3-yl)-1-{(S)-4-methyl-2-[3-(1-methyl-cyclohexyl)-ureido]-pentanoylamino}-ethyl)-oxazole-4-carboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10percent Pd/C / ethanol / 4 h / Ambient temperature

2: 1-ethyl-3-(3-(dimethylamino)propyl)carbodiimide hydrochloride, 1-hydroxybenzotriazole hydrate, N-methylmorpholine / tetrahydrofuran; dimethylformamide

With 4-methyl-morpholine; hydrogen; 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm950592+