Technology Process of C12H5BrF3N3O2S
There total 4 articles about C12H5BrF3N3O2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine; pyridine N-oxide; oxygen; copper diacetate;
In
dichloromethane;
at 20 ℃;
for 12h;
Molecular sieve;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: thionyl chloride / 5 h / 100 °C
2: hydrogenchloride; dihydrogen peroxide / water / 0.25 h / 100 °C / Microwave irradiation
3: copper diacetate; pyridine N-oxide; pyridine; oxygen / dichloromethane / 12 h / 20 °C / Molecular sieve
With
pyridine; pyridine N-oxide; hydrogenchloride; thionyl chloride; dihydrogen peroxide; oxygen; copper diacetate;
In
dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogen bromide; bromine / 5 h / 40 - 110 °C
2: thionyl chloride / 5 h / 100 °C
3: hydrogenchloride; dihydrogen peroxide / water / 0.25 h / 100 °C / Microwave irradiation
4: copper diacetate; pyridine N-oxide; pyridine; oxygen / dichloromethane / 12 h / 20 °C / Molecular sieve
With
pyridine; pyridine N-oxide; hydrogenchloride; thionyl chloride; hydrogen bromide; dihydrogen peroxide; bromine; oxygen; copper diacetate;
In
dichloromethane; water;