8-azidooctyl 2,6-di-O-benzoyl-4-O-levulinoyl-3-O-methyl-α-D-mannopyranosyl-(1→4)-2,6-di-O-benzoyl-3-O-methyl-α-D-mannopyranoside

Base Information

Chemical Name:8-azidooctyl 2,6-di-O-benzoyl-4-O-levulinoyl-3-O-methyl-α-D-mannopyranosyl-(1→4)-2,6-di-O-benzoyl-3-O-methyl-α-D-mannopyranoside
CAS No.:1408060-42-3
Molecular Formula:C₅₅H₆₃N₃O₁₇
Molecular Weight:1038.12
Hs Code.:

Synonyms:8-azidooctyl 2,6-di-O-benzoyl-4-O-levulinoyl-3-O-methyl-α-D-mannopyranosyl-(1→4)-2,6-di-O-benzoyl-3-O-methyl-α-D-mannopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-azidooctyl 2,6-di-O-benzoyl-4-O-levulinoyl-3-O-methyl-α-D-mannopyranosyl-(1→4)-2,6-di-O-benzoyl-3-O-methyl-α-D-mannopyranoside

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Technology Process of 8-azidooctyl 2,6-di-O-benzoyl-4-O-levulinoyl-3-O-methyl-α-D-mannopyranosyl-(1→4)-2,6-di-O-benzoyl-3-O-methyl-α-D-mannopyranoside

There total 6 articles about 8-azidooctyl 2,6-di-O-benzoyl-4-O-levulinoyl-3-O-methyl-α-D-mannopyranosyl-(1→4)-2,6-di-O-benzoyl-3-O-methyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1408060-40-1
ethyl 2,6-di-O-benzoyl-4-O-levulinoyl-3-O-methyl-α-D-mannopyranosyl-(1→4)-2,6-di-O-benzoyl-3-O-methyl-1-thio-α-D-mannopyranoside

: 57395-46-7
8-azidooctan-1-ol

: 1408060-42-3
8-azidooctyl 2,6-di-O-benzoyl-4-O-levulinoyl-3-O-methyl-α-D-mannopyranosyl-(1→4)-2,6-di-O-benzoyl-3-O-methyl-α-D-mannopyranoside

Guidance literature:: With N-iodo-succinimide; silver trifluoromethanesulfonate; In dichloromethane; at 0 - 20 ℃; Inert atmosphere; Molecular sieve;
DOI:10.1002/chem.201201222 DOI:10.1002/chem.201201222

Reference yield:

: 1408060-54-7
ethyl 3-O-methyl-1-thio-α-D-mannopyranoside

: 1408060-42-3
8-azidooctyl 2,6-di-O-benzoyl-4-O-levulinoyl-3-O-methyl-α-D-mannopyranosyl-(1→4)-2,6-di-O-benzoyl-3-O-methyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / dichloromethane / 17 h / -20 - 20 °C / Inert atmosphere

2: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

3: N-iodo-succinimide; silver trifluoromethanesulfonate / dichloromethane / 0 - 20 °C / Inert atmosphere; Molecular sieve

With pyridine; N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; silver trifluoromethanesulfonate; In dichloromethane;
DOI:10.1002/chem.201201222 DOI:10.1002/chem.201201222

Reference yield:

: 1408060-55-8
ethyl 2,6-di-O-benzoyl-3-O-methyl-1-thio-α-D-mannopyranoside

: 1408060-42-3
8-azidooctyl 2,6-di-O-benzoyl-4-O-levulinoyl-3-O-methyl-α-D-mannopyranosyl-(1→4)-2,6-di-O-benzoyl-3-O-methyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

2: N-iodo-succinimide; silver trifluoromethanesulfonate / dichloromethane / 0 - 20 °C / Inert atmosphere; Molecular sieve

With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; silver trifluoromethanesulfonate; In dichloromethane;
DOI:10.1002/chem.201201222 DOI:10.1002/chem.201201222