4-[α-hydroxy-α-(1-tricyclo[3.3.1.1^3,7]decyl)phenylmethyl]benzenepropanol

Base Information

Chemical Name:4-[α-hydroxy-α-(1-tricyclo[3.3.1.1^3,7]decyl)phenylmethyl]benzenepropanol
CAS No.:1410789-83-1
Molecular Formula:C₂₆H₃₂O₂
Molecular Weight:376.539
Hs Code.:

4-[α-hydroxy-α-(1-tricyclo[3.3.1.1<sup>3,7</sup>]decyl)phenylmethyl]benzenepropanol

Synonyms:4-[α-hydroxy-α-(1-tricyclo[3.3.1.1^3,7]decyl)phenylmethyl]benzenepropanol

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Chemical Property of 4-[α-hydroxy-α-(1-tricyclo[3.3.1.1^3,7]decyl)phenylmethyl]benzenepropanol

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Technology Process of 4-[α-hydroxy-α-(1-tricyclo[3.3.1.1^3,7]decyl)phenylmethyl]benzenepropanol

There total 3 articles about 4-[α-hydroxy-α-(1-tricyclo[3.3.1.1^3,7]decyl)phenylmethyl]benzenepropanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: α-phenyl-α-[4-(2-propenyl)pheny]-1-tricyclo-[3.3.1.1^3,7]decanemethanol

: 1410789-83-1
4-[α-hydroxy-α-(1-tricyclo[3.3.1.1^3,7]decyl)phenylmethyl]benzenepropanol

Guidance literature:: α-phenyl-α-[4-(2-propenyl)pheny]-1-tricyclo-[3.3.1.1^3,7]decanemethanol; With borane-THF; In tetrahydrofuran; at 0 - 20 ℃; for 3h; Inert atmosphere;

With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; at 50 - 60 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jm3013008

Reference yield:

: 2294-43-1
1-allyl-4-bromo-benzene

: 1410789-83-1
4-[α-hydroxy-α-(1-tricyclo[3.3.1.1^3,7]decyl)phenylmethyl]benzenepropanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: magnesium / tetrahydrofuran / 3 h / 40 °C / Inert atmosphere

2.1: borane-THF / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere

2.2: 1 h / 50 - 60 °C / Inert atmosphere

With borane-THF; magnesium; In tetrahydrofuran;
DOI:10.1021/jm3013008

Reference yield:

: 31919-47-8
1-benzoyladamantane

: 1410789-83-1
4-[α-hydroxy-α-(1-tricyclo[3.3.1.1^3,7]decyl)phenylmethyl]benzenepropanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: magnesium / tetrahydrofuran / 3 h / 40 °C / Inert atmosphere

2.1: borane-THF / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere

2.2: 1 h / 50 - 60 °C / Inert atmosphere

With borane-THF; magnesium; In tetrahydrofuran;
DOI:10.1021/jm3013008