(2S,3R,4R,5R)-2,3,5-Tris-(tert-butyl-dimethyl-silanyloxy)-6-(tert-butyl-diphenyl-silanyloxy)-4-methoxymethoxy-hexanal

Base Information

Chemical Name:(2S,3R,4R,5R)-2,3,5-Tris-(tert-butyl-dimethyl-silanyloxy)-6-(tert-butyl-diphenyl-silanyloxy)-4-methoxymethoxy-hexanal
CAS No.:184691-08-5
Molecular Formula:C₄₂H₇₆O₇Si₄
Molecular Weight:805.403
Hs Code.:

Synonyms:(2S,3R,4R,5R)-2,3,5-Tris-(tert-butyl-dimethyl-silanyloxy)-6-(tert-butyl-diphenyl-silanyloxy)-4-methoxymethoxy-hexanal

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Chemical Property of (2S,3R,4R,5R)-2,3,5-Tris-(tert-butyl-dimethyl-silanyloxy)-6-(tert-butyl-diphenyl-silanyloxy)-4-methoxymethoxy-hexanal

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Technology Process of (2S,3R,4R,5R)-2,3,5-Tris-(tert-butyl-dimethyl-silanyloxy)-6-(tert-butyl-diphenyl-silanyloxy)-4-methoxymethoxy-hexanal

There total 4 articles about (2S,3R,4R,5R)-2,3,5-Tris-(tert-butyl-dimethyl-silanyloxy)-6-(tert-butyl-diphenyl-silanyloxy)-4-methoxymethoxy-hexanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 184691-07-4
C₄₄H₈₀O₆Si₄

: 184691-08-5
(2S,3R,4R,5R)-2,3,5-Tris-(tert-butyl-dimethyl-silanyloxy)-6-(tert-butyl-diphenyl-silanyloxy)-4-methoxymethoxy-hexanal

Guidance literature:: With dimethylsulfide; ozone;
DOI:10.1021/jo961671b

Reference yield:

: 184691-04-1
C₃₀H₄₈O₄Si₂

: 184691-08-5
(2S,3R,4R,5R)-2,3,5-Tris-(tert-butyl-dimethyl-silanyloxy)-6-(tert-butyl-diphenyl-silanyloxy)-4-methoxymethoxy-hexanal

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / O₃, Me₂S

2: 37 percent / BF₃*OEt₂

3: 82 percent / 2,6-lutidine / CH₂Cl₂ / 0.67 h / 0 °C

4: 91 percent / O₃, Me₂S

With 2,6-dimethylpyridine; dimethylsulfide; boron trifluoride diethyl etherate; ozone; In dichloromethane;
DOI:10.1021/jo961671b

Reference yield:

: 184691-05-2
(2R,3R)-3-(tert-Butyl-dimethyl-silanyloxy)-4-(tert-butyl-diphenyl-silanyloxy)-2-methoxymethoxy-butyraldehyde

: 184691-08-5
(2S,3R,4R,5R)-2,3,5-Tris-(tert-butyl-dimethyl-silanyloxy)-6-(tert-butyl-diphenyl-silanyloxy)-4-methoxymethoxy-hexanal

Guidance literature:: Multi-step reaction with 3 steps

1: 37 percent / BF₃*OEt₂

2: 82 percent / 2,6-lutidine / CH₂Cl₂ / 0.67 h / 0 °C

3: 91 percent / O₃, Me₂S

With 2,6-dimethylpyridine; dimethylsulfide; boron trifluoride diethyl etherate; ozone; In dichloromethane;
DOI:10.1021/jo961671b