benzyl (Rs)-4-(tert-butyldimethylsiloxy)-3-hydroxy-2-(p-tolylsulfinyl)butanoate

Base Information

Chemical Name:benzyl (Rs)-4-(tert-butyldimethylsiloxy)-3-hydroxy-2-(p-tolylsulfinyl)butanoate
CAS No.:1166835-69-3
Molecular Formula:C₂₄H₃₄O₅SSi
Molecular Weight:462.682
Hs Code.:

Synonyms:benzyl (Rs)-4-(tert-butyldimethylsiloxy)-3-hydroxy-2-(p-tolylsulfinyl)butanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl (Rs)-4-(tert-butyldimethylsiloxy)-3-hydroxy-2-(p-tolylsulfinyl)butanoate

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Technology Process of benzyl (Rs)-4-(tert-butyldimethylsiloxy)-3-hydroxy-2-(p-tolylsulfinyl)butanoate

There total 1 articles about benzyl (Rs)-4-(tert-butyldimethylsiloxy)-3-hydroxy-2-(p-tolylsulfinyl)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 102191-92-4
tert-butyldimethylsiloxyacetaldehyde

: 148871-73-2
benzyl (R)-(+)-(p-tolylsulfinyl)acetate

: 1166835-69-3
benzyl (Rs)-4-(tert-butyldimethylsiloxy)-3-hydroxy-2-(p-tolylsulfinyl)butanoate

Guidance literature:: benzyl (R)-(+)-(p-tolylsulfinyl)acetate; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.5h;

tert-butyldimethylsiloxyacetaldehyde; In tetrahydrofuran; at -78 ℃; for 2.5h;
DOI:10.1055/s-0028-1088008

Reference yield:

: 1166835-69-3
benzyl (Rs)-4-(tert-butyldimethylsiloxy)-3-hydroxy-2-(p-tolylsulfinyl)butanoate

: C₁₇H₂₈O₅SSi

Guidance literature:: With 10% palladium on activated carbon; hydrogen; In ethyl acetate; at 25 ℃; for 4h; under 760.051 Torr;
DOI:10.1055/s-0028-1088008