N⁹-(4'-bis(POM)-phosphinylbut-2'-enyl)-2-amino-6-(4-isopropyl)phenylaminopurine

Base Information

Chemical Name:N⁹-(4'-bis(POM)-phosphinylbut-2'-enyl)-2-amino-6-(4-isopropyl)phenylaminopurine
CAS No.:1365349-54-7
Molecular Formula:C₃₀H₄₃N₆O₇P
Molecular Weight:630.681
Hs Code.:

N<SUP>9</SUP>-(4'-bis(POM)-phosphinylbut-2'-enyl)-2-amino-6-(4-isopropyl)phenylaminopurine

Synonyms:N⁹-(4'-bis(POM)-phosphinylbut-2'-enyl)-2-amino-6-(4-isopropyl)phenylaminopurine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N⁹-(4'-bis(POM)-phosphinylbut-2'-enyl)-2-amino-6-(4-isopropyl)phenylaminopurine

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Technology Process of N⁹-(4'-bis(POM)-phosphinylbut-2'-enyl)-2-amino-6-(4-isopropyl)phenylaminopurine

There total 5 articles about N⁹-(4'-bis(POM)-phosphinylbut-2'-enyl)-2-amino-6-(4-isopropyl)phenylaminopurine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 929837-29-6
2-amino-6-(4-isopropyl)phenylaminopurine

: 1415634-04-6
(E)-bis(POM)-4-hydroxy-but-2-en-1-yl phosphonate

: 1365349-54-7
N⁹-(4'-bis(POM)-phosphinylbut-2'-enyl)-2-amino-6-(4-isopropyl)phenylaminopurine

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In 1,4-dioxane; at 10 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.ejmech.2012.08.042

Reference yield: 45.0%

: 1365349-54-7
N⁹-(4'-bis(POM)-phosphinylbut-2'-enyl)-2-amino-6-(4-isopropyl)phenylaminopurine

Guidance literature:

Reference yield:

: 1258789-63-7
[({[(2,2-dimethylpropanoyl)oxy]methoxy}(prop-2-en-1-yl)phosphoryl)oxy]methyl 2,2-dimethylpropanoate

: 1365349-54-7
N⁹-(4'-bis(POM)-phosphinylbut-2'-enyl)-2-amino-6-(4-isopropyl)phenylaminopurine

Guidance literature:: Multi-step reaction with 2 steps

1: [1,3-bis(2,4,6-trimethylphenyl)-2-imidazolidinylidene]dichloro(phenylmethylene)(triphenylphosphine)ruthenium(II) / dichloromethane / 48 h / 40 °C / Inert atmosphere

2: triphenylphosphine; di-isopropyl azodicarboxylate / 1,4-dioxane / 10 - 20 °C / Inert atmosphere

With [1,3-bis(2,4,6-trimethylphenyl)-2-imidazolidinylidene]dichloro(phenylmethylene)(triphenylphosphine)ruthenium(II); di-isopropyl azodicarboxylate; triphenylphosphine; In 1,4-dioxane; dichloromethane; 2: |Mitsunobu Displacement;
DOI:10.1016/j.ejmech.2012.08.042