N,N'-[bis(3-benzyloxy-1,4-dihydro-2-methyl-4-oxo-1-pyridyl)hexanoyl]-1,5-diamino-3-oxapentane

Base Information

Chemical Name:N,N'-[bis(3-benzyloxy-1,4-dihydro-2-methyl-4-oxo-1-pyridyl)hexanoyl]-1,5-diamino-3-oxapentane
CAS No.:573968-08-8
Molecular Formula:C₄₂H₅₄N₄O₇
Molecular Weight:726.913
Hs Code.:

Synonyms:N,N'-[bis(3-benzyloxy-1,4-dihydro-2-methyl-4-oxo-1-pyridyl)hexanoyl]-1,5-diamino-3-oxapentane

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Chemical Property of N,N'-[bis(3-benzyloxy-1,4-dihydro-2-methyl-4-oxo-1-pyridyl)hexanoyl]-1,5-diamino-3-oxapentane

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Technology Process of N,N'-[bis(3-benzyloxy-1,4-dihydro-2-methyl-4-oxo-1-pyridyl)hexanoyl]-1,5-diamino-3-oxapentane

There total 3 articles about N,N'-[bis(3-benzyloxy-1,4-dihydro-2-methyl-4-oxo-1-pyridyl)hexanoyl]-1,5-diamino-3-oxapentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 2752-17-2
2,2'-diaminodiethyl ether

: 99110-60-8
3-benzyloxy-1-carboxypentyl-2-methyl-4(1H)-pyridinone

: 573968-08-8
N,N'-[bis(3-benzyloxy-1,4-dihydro-2-methyl-4-oxo-1-pyridyl)hexanoyl]-1,5-diamino-3-oxapentane

Guidance literature:: With 1,1'-carbonyldiimidazole; In N,N-dimethyl-formamide; at 40 ℃; for 120h;
DOI:10.3987/COM-03-9719

Reference yield:

: 61049-69-2
3-O-benzylmaltol

: 573968-08-8
N,N'-[bis(3-benzyloxy-1,4-dihydro-2-methyl-4-oxo-1-pyridyl)hexanoyl]-1,5-diamino-3-oxapentane

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / aq. NaOH / aq. ethanol / 48 h / Heating

2: 44 percent / N,N'-carbonyldiimidazole / dimethylformamide / 120 h / 40 °C

With sodium hydroxide; 1,1'-carbonyldiimidazole; In ethanol; N,N-dimethyl-formamide;
DOI:10.3987/COM-03-9719

Reference yield:

: 60-32-2,93208-38-9
6-aminohexanoic acid

: 573968-08-8
N,N'-[bis(3-benzyloxy-1,4-dihydro-2-methyl-4-oxo-1-pyridyl)hexanoyl]-1,5-diamino-3-oxapentane

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / aq. NaOH / aq. ethanol / 48 h / Heating

2: 44 percent / N,N'-carbonyldiimidazole / dimethylformamide / 120 h / 40 °C

With sodium hydroxide; 1,1'-carbonyldiimidazole; In ethanol; N,N-dimethyl-formamide;
DOI:10.3987/COM-03-9719