C₁₀H₁₀ClFO₄S

Base Information

Chemical Name:C₁₀H₁₀ClFO₄S
CAS No.:1402743-27-4
Molecular Formula:C₁₀H₁₀ClFO₄S
Molecular Weight:280.704
Hs Code.:

C<sub>10</sub>H<sub>10</sub>ClFO<sub>4</sub>S

Synonyms:C₁₀H₁₀ClFO₄S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₀H₁₀ClFO₄S

Chemical Property:

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Technology Process of C₁₀H₁₀ClFO₄S

There total 2 articles about C₁₀H₁₀ClFO₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1402743-26-3
C₁₀H₁₁FO₅S

: 1402743-27-4
C₁₀H₁₀ClFO₄S

Guidance literature:: With thionyl chloride; for 3h; Reflux;

Reference yield:

: 1402743-25-2
methyl 2-(2-fluorophenyl)acrylate

: 1402743-27-4
C₁₀H₁₀ClFO₄S

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogensulfite / ethanol; water / 0.5 h / 165 °C / microwave reactor

2: thionyl chloride / 3 h / Reflux

With thionyl chloride; sodium hydrogensulfite; In ethanol; water;

Reference yield:

: 1402743-27-4
C₁₀H₁₀ClFO₄S

: C₂₀H₂₅FN₂O₄S

Guidance literature:: Multi-step reaction with 8 steps

1.1: triethylamine / dichloromethane / 3 h / 0 - 25 °C

2.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C

3.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C

3.2: 8 h / -78 - 25 °C

4.1: ozone / dichloromethane / -78 °C

4.2: -78 - 25 °C

5.1: hydrogen / palladium on activated charcoal / ethanol / 760.05 Torr

6.1: diethoxyltriphenylphosphorane / toluene / 60 h / 45 °C

7.1: water; lithium hydroxide / tetrahydrofuran / 25 - 60 °C

7.2: pH 3

8.1: triethylamine; diphenyl phosphoryl azide / tetrahydrofuran / 24 h / 25 °C

8.2: 1.5 h / 80 °C

With diphenyl phosphoryl azide; diethoxyltriphenylphosphorane; water; hydrogen; ozone; triethylamine; lithium hydroxide; lithium diisopropyl amide; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; toluene;